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[ CAS No. 16966-09-9 ] {[proInfo.proName]}

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Chemical Structure| 16966-09-9
Chemical Structure| 16966-09-9
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Product Details of [ 16966-09-9 ]

CAS No. :16966-09-9 MDL No. :MFCD06248909
Formula : C16H23NO5 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 309.36 Pubchem ID :-
Synonyms :

Safety of [ 16966-09-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 16966-09-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 16966-09-9 ]
  • Downstream synthetic route of [ 16966-09-9 ]

[ 16966-09-9 ] Synthesis Path-Upstream   1~12

  • 1
  • [ 16966-09-9 ]
  • [ 4378-13-6 ]
Reference: [1] Bulletin of the Chemical Society of Japan, 1982, vol. 55, # 9, p. 3049 - 3050
  • 2
  • [ 52785-41-8 ]
  • [ 16966-09-9 ]
YieldReaction ConditionsOperation in experiment
80.3% With sodium hydroxide In water; acetone 4The Z-thr (tbu) -ome 169g was added to 2L beaker, 300Ml of acetone 600Ml, 2mlc / l sodium hydroxide adjusted to pH 10-11 reaction. The reaction is completed, washed with ether 500ml once, add ethyl acetate 800ml, citric acid aqueous solution to adjust the pH in 2-3.300ml washed, 300ml saturated salt water wash. 100G dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to dry granulated ether 500ML to give z-thr (tbu) -oH 130 g, yield 80.3percent
Reference: [1] Patent: CN106631900, 2017, A, . Location in patent: Paragraph 0015
[2] Justus Liebigs Annalen der Chemie, 1963, vol. 670, p. 127 - 136
[3] Bulletin of the Chemical Society of Japan, 1982, vol. 55, # 9, p. 3049 - 3050
  • 3
  • [ 57224-63-2 ]
  • [ 16966-09-9 ]
Reference: [1] Bulletin of the Chemical Society of Japan, 1982, vol. 55, # 9, p. 3049 - 3050
[2] Justus Liebigs Annalen der Chemie, 1963, vol. 670, p. 127 - 136
[3] Patent: CN106631900, 2017, A,
  • 4
  • [ 83824-81-1 ]
  • [ 16966-09-9 ]
Reference: [1] Bulletin of the Chemical Society of Japan, 1982, vol. 55, # 9, p. 3049 - 3050
  • 5
  • [ 14437-51-5 ]
  • [ 16966-09-9 ]
Reference: [1] Synthesis, 1996, # 12, p. 1433 - 1434
  • 6
  • [ 16879-87-1 ]
  • [ 16966-09-9 ]
Reference: [1] Chemische Berichte, 1964, vol. 97, p. 2490 - 2496
  • 7
  • [ 16879-84-8 ]
  • [ 16966-09-9 ]
Reference: [1] Chemische Berichte, 1964, vol. 97, p. 2490 - 2496
  • 8
  • [ 19728-63-3 ]
  • [ 16966-09-9 ]
Reference: [1] Chemische Berichte, 1964, vol. 97, p. 2490 - 2496
  • 9
  • [ 501-53-1 ]
  • [ 16966-09-9 ]
Reference: [1] Patent: CN106631900, 2017, A,
  • 10
  • [ 16966-07-7 ]
  • [ 16966-09-9 ]
Reference: [1] Tetrahedron, 1980, vol. 36, # 90, p. 2241 - 2245
  • 11
  • [ 16966-09-9 ]
  • [ 101-83-7 ]
  • [ 16966-07-7 ]
Reference: [1] Synthesis (Germany), 2014, vol. 46, # 22, p. 3075 - 3084
  • 12
  • [ 16966-09-9 ]
  • [ 189337-28-8 ]
Reference: [1] Patent: CN106631900, 2017, A,
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