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CAS No. : | 10228-54-3 | MDL No. : | |
Formula : | C7H14O3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 146.18 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With potassium hydroxide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
General procedure: To a solution of <strong>[1404-90-6]vancomycin</strong> (0.74 g, 0.5 mmol, 1 equiv) in 40 mL of anhydrous DMF was added 1a (150 mg, 0.6 mmol, 1.2 equiv). The mixture was stirred at 80 C for 2 h until HPLC indicated the disappearance of <strong>[1404-90-6]vancomycin</strong>. To the mixture was added AcOH (8 mL) and NaBH3CN (63 mg, 1.0 mmol, 2 equiv). The reaction was stirred for another 2 h. The reaction mixture was directly subjected to preparative reverse phase HPLC purification to give product 6a (508 mg, 62% yield) as a white solid. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With thionyl chloride |