Home Cart 0 Sign in  

[ CAS No. 1036959-27-9 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
Chemical Structure| 1036959-27-9
Chemical Structure| 1036959-27-9
Structure of 1036959-27-9 * Storage: {[proInfo.prStorage]}
Cart0 Add to My Favorites Add to My Favorites Bulk Inquiry Inquiry Add To Cart

Quality Control of [ 1036959-27-9 ]

Related Doc. of [ 1036959-27-9 ]

Alternatived Products of [ 1036959-27-9 ]

Product Details of [ 1036959-27-9 ]

CAS No. :1036959-27-9 MDL No. :
Formula : C17H25N3O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 303.40 Pubchem ID :-
Synonyms :
(2R)-LAF237;(2R)-NVP-LAF 237

Safety of [ 1036959-27-9 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 1036959-27-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1036959-27-9 ]

[ 1036959-27-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 702-82-9 ]
  • [ 207557-35-5 ]
  • [ 1036959-27-9 ]
YieldReaction ConditionsOperation in experiment
85% With potassium carbonate; potassium iodide; In butanone; at 70℃; for 1h; 1) A mixed solution of 3-amino-1-adamantanol and 1-chloroacetyl-2-cyanopyrrolidine in a solvent was mixed with a suspension of a base and a catalyst and then preheated by a preheater;2) The preheated mixture enters the tubular reactor, the residence time of the material in the tubular reactor is 60min, and then the reaction liquid withdrawn from the tubular reactor is collected and filtered, washed and purified to obtain the product.The process parameters are as follows:The preheater temperature is 70 C, the tube reactor temperature is 70 C, and the flow rate of the material in the line is 0.5 m / s.The molar ratio of 3-amino-1-adamantanol to 1-chloroacetyl-2-cyanopyrrolidine was 2: 1,3-amino-1-adamantanol was 0.13 g / ml, 1-chloro The concentration of acetyl-2-cyanopyrrolidine was 0.068 g / ml, the molar ratio of potassium carbonate to 1-chloroacetyl-2-cyanopyrrolidine was 1: 1, the amount of potassium iodide was the same as that of 1-chloroacetyl The molar ratio of 2-cyanopyrrolidine was 0.5: 1, and the reaction solvent was 2-butanone.Under this operating condition, the yield of the Viglitin reaction was 85% and the amount of the disubstituted compound was 4.5%.
Same Skeleton Products
Historical Records