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CAS No. : | 1050602-55-5 | MDL No. : | |
Formula : | C7H7Cl2N3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 204.06 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
35% | With hydrogenchloride; In 1,4-dioxane; acetonitrile; at 85℃; for 16h; | At room temperature, 400 mul of a 4 M solution of HCl in dioxane are added to a solution of 218 mg (1.00 mmol) of 2,5-dichloro-N-(cyclopropylmethyl)pyrimidine-4-amine and 299 mg (1.98 mmol) of <strong>[7664-66-6]4-(isopropoxy)aniline</strong> in 12 ml of acetonitrile, and the mixture is heated at 85 C. After 16 h, the hot reaction mixture is filtered and the filtrate is allowed to cool with stirring. The product precipitated from the filtrate is filtered off and dried. This gives 130 mg (35%). logP (pH2.3): 2.11 |