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[ CAS No. 1060651-05-9 ] {[proInfo.proName]}

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Chemical Structure| 1060651-05-9
Chemical Structure| 1060651-05-9
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Quality Control of [ 1060651-05-9 ]

COA NMR CNMR HPLC LC-MS

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Product Details of [ 1060651-05-9 ]

CAS No. :1060651-05-9 MDL No. :MFCD31630414
Formula : C27H36N2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 404.60 Pubchem ID :-
Synonyms :

Safety of [ 1060651-05-9 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1060651-05-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1060651-05-9 ]

[ 1060651-05-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 578743-87-0 ]
  • [ 1060651-05-9 ]
YieldReaction ConditionsOperation in experiment
18 mg With N,N-dimethyl-formamide; potassium (trifluoromethyl)trimethoxyborate; at 30℃; for 10h;Inert atmosphere; General procedure: To a stirred solution of imidazolium salts (0.045 mmol), NaOtBu (4.3 mg, 0.045 mmol) and CuCl (4.5mg, 0.045 mmol) was added THF (0.5 mL, 0.09 M) at 30 oC under argon atmosphere. After stirring for 2 h, the solution of K+[CF3B(OMe)3]- (63.5 mg, 0.3 mmol, 6.0 equiv) in DMF (0.5 mL) was added dropwise. Then the mixture was kept stirring at 30 oC for 10 h. After that, the reaction was quenched with water. Aqueous layer was extracted with EtOAc (15 mL x 3), and the combined organic layers was washed with brine, dried over Na2SO4 and concentrated under reduced pressure. Then the crude product was purified by column chromatography on silica gel to give the imidazolinone 3b-d.
Reference： [1]Journal of Organometallic Chemistry,2013,vol. 743,p. 44 - 48
[2]Journal of Organometallic Chemistry,2013,vol. 743,p. 44 - 48
[3]Journal of Organometallic Chemistry,2013,vol. 743,p. 44 - 48
  • 2
  • [ 578743-87-0 ]
  • [ 1060651-05-9 ]
  • [ 250285-32-6 ]
YieldReaction ConditionsOperation in experiment
16%Spectr.; 81%Spectr. With water; oxygen; In dimethylsulfoxide-d6; at 150℃; for 155h;Sealed tube;Kinetics; General procedure: Cu(I)-NHC 1a-g (0.04 mmol, 1.0 equiv) and CDCl3 (0.4 mL, degassed by bubbling argon for 30 min) were added into a flame-dried NMR tube. (CD3)2SO (0.4 mL) was used for 1h (0.04 mmol), 1i (0.02 mmol), and 1j (0.02 mmol). The NMR tube was closed with a septum and equipped with an air balloon (approximate 500 mL) containing approximately 100 mL of O2 (4.5 mmol, 112 equiv.) and approximately 12.6 mL of H2O (gas, 0.56 mmol, 14 equiv., air relative humidity = 75%). The solution (not agitated) was placed at room temperature and was monitored by 1H NMR. 100 C was used for the decomposition of 1h, and 150 C was used for the decomposition of 1i and 1j. The precipitate in the NMR tube was removed by quick filtration using a membrane filter before each 1H NMR measurement. The ratio of Cu-NHC, urea, and imidazolium were calculated through the integration of 1H NMR, using the normalization method. The characterization of products could be found in the previous study [32].
Reference： [1]Organic Letters,2019,vol. 21,p. 3572 - 3575
[2]Journal of Organometallic Chemistry,2020,vol. 906

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