Alternatived Products of [ 1116122-85-0 ]
Product Details of [ 1116122-85-0 ]
CAS No. : | 1116122-85-0 |
MDL No. : | MFCD25460334 |
Formula : |
C26H32B2N2O5
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
474.17
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 1116122-85-0 ]
Application In Synthesis of [ 1116122-85-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1116122-85-0 ]
- 1
-
[ 19542-05-3 ]
-
[ 73183-34-3 ]
-
[ 1116122-85-0 ]
Yield | Reaction Conditions | Operation in experiment |
84% |
With KCH3COO In 1,4-dioxane (N2); bis(pinacolato)diboron, Pd complex and KCH3COO added to a soln. of(BrC6H4)2C2N2O, stirred at 100°C; cooled, evapd. (vac.), CH2Cl2 and H2O added, extd. (CH2Cl2, twice), the org. layer washed with H2O and brine, dried (MgSO4), evapd. (vac.), chromd. (silica gel, CH2Cl2/hexane, EtOAc/hexane); elem. anal.; |
|
84% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane at 100℃; Inert atmosphere; |
|
|
With potassium acetate In 1,4-dioxane |
|
Reference:
[1]Lee, Taegweon; Landis, Chad A.; Dhar, Bal Mukund; Jung, Byung Jun; Sun, Jia; et al.
[Journal of the American Chemical Society, 2009, vol. 131, p. 1692 - 1705]
[2]Location in patent: experimental part
Lee, Taegweon; Landis, Chad A.; Dhar, Bal Mukund; Jung, Byung Jun; Sun, Jia; et al.
[Journal of the American Chemical Society, 2009, vol. 131, p. 1692 - 1705]
[3]Hao, Zhaoran; Li, Min; Liu, Yajun; Wang, Yafei; Xie, Guohua; Liu, Yu
[Dyes and Pigments, 2018, vol. 149, p. 315 - 322]