Alternatived Products of [ 1127-49-7 ]
Product Details of [ 1127-49-7 ]
CAS No. : | 1127-49-7 |
MDL No. : | MFCD07528159 |
Formula : |
C9H9N3
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
159.19
|
Pubchem ID : | - |
Synonyms : |
|
Application In Synthesis of [ 1127-49-7 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1127-49-7 ]
- 1
-
[ 607-32-9 ]
-
[ 1127-49-7 ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 2 steps
1: 87 percent / hydroxylamine hydrochloride; NaOH / aq. ethanol; methanol / 1.5 h / 50 - 60 °C
2: 95 percent / H2 / Pd-C / aq. ethanol / 2 h / 1551.44 Torr |
|
|
Multi-step reaction with 2 steps
1: 87 percent / HONH2, KOH / ethanol / 5 h / 60 °C
2: 95 percent / H2 / 10 percent Pd/C / ethanol / 4 h / 1551.44 Torr / Ambient temperature |
|
|
Multi-step reaction with 2 steps
1: 79 percent / activated carbon, FeCl3*6H2O, hydrazine / methanol / 16 h / Heating
2: 1.) Na2CO3, diazotized sulfanilic acid, 2.) sodium hydroxide, sodium dithionite / 1.) AcOH, 7-9 deg C, 30 min, 2.) water, 60 deg C, 30 min |
|
Reference:
[1]Ryu, Chung-Kyu; Lee, In-Kyung; Jung, Sung-Hee; Kang, Hye-Young; Lee, Chong-Ock
[Medicinal Chemistry Research, 2000, vol. 10, # 1, p. 40 - 49]
[2]Ryu, Chung-Kyu; Lee, In-Kyung; Jung, Sung-Hee; Lee, Chong-Ock
[Bioorganic and Medicinal Chemistry Letters, 1999, vol. 9, # 8, p. 1075 - 1080]
[3]Potts, Kevin T.; Bhattacharjee, Debkumar; Walsh, Eileen B.
[Journal of Organic Chemistry, 1986, vol. 51, # 11, p. 2011 - 2021]