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CAS No. : | 1162697-10-0 | MDL No. : | MFCD21219877 |
Formula : | C11H15BrN2O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 271.15 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | N/A | |
Precautionary Statements: | UN#: | N/A | |
Hazard Statements: | Packing Group: | N/A |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
201 mg | at 100℃; for 12 h; | To a solution of compound 5-bromo-Nl-(tetrahydro-2H-pyran-4-yl)benzene-l,2- diamine (500 mg, 1.852 mmol) in HC(OMe)3 (2 mL) was added TsOH (15mg, 0.0789 mmol). The reaction mixture was stirred at 100 °C for 12h. The reaction mixture was extracted with DCM washed with water and the organic layer dried over sodium sulfate which was removed by filtration. After concentration of the filtrate, the crude product was purified by column (201 mg, 38.53percent). LCMS (m/z): 281.0, 283.0 (M+l). |