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[ CAS No. 1162697-10-0 ] {[proInfo.proName]}

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Chemical Structure| 1162697-10-0
Chemical Structure| 1162697-10-0
Structure of 1162697-10-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1162697-10-0 ]

CAS No. :1162697-10-0 MDL No. :MFCD21219877
Formula : C11H15BrN2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 271.15 Pubchem ID :-
Synonyms :

Safety of [ 1162697-10-0 ]

Signal Word: Class:N/A
Precautionary Statements: UN#:N/A
Hazard Statements: Packing Group:N/A

Application In Synthesis of [ 1162697-10-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 1162697-10-0 ]
  • Downstream synthetic route of [ 1162697-10-0 ]

[ 1162697-10-0 ] Synthesis Path-Upstream   1~2

  • 1
  • [ 1162697-10-0 ]
  • [ 149-73-5 ]
  • [ 1245649-58-4 ]
YieldReaction ConditionsOperation in experiment
201 mg at 100℃; for 12 h; To a solution of compound 5-bromo-Nl-(tetrahydro-2H-pyran-4-yl)benzene-l,2- diamine (500 mg, 1.852 mmol) in HC(OMe)3 (2 mL) was added TsOH (15mg, 0.0789 mmol). The reaction mixture was stirred at 100 °C for 12h. The reaction mixture was extracted with DCM washed with water and the organic layer dried over sodium sulfate which was removed by filtration. After concentration of the filtrate, the crude product was purified by column (201 mg, 38.53percent). LCMS (m/z): 281.0, 283.0 (M+l).
Reference: [1] Patent: WO2014/100695, 2014, A1, . Location in patent: Paragraph 00344
  • 2
  • [ 64-18-6 ]
  • [ 1162697-10-0 ]
  • [ 1245649-58-4 ]
Reference: [1] Patent: WO2014/151147, 2014, A1, . Location in patent: Paragraph 00641
[2] Patent: US2015/30588, 2015, A1, . Location in patent: Page/Page column 71; 72
[3] Patent: US9295673, 2016, B2, . Location in patent: Page/Page column 352; 353
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