There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
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CAS No. : | 1210-96-4 | MDL No. : | MFCD00454170 |
Formula : | C8H8N2O6 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 228.16 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Danger | Class: | 4.1,6.1 |
Precautionary Statements: | P240-P210-P241-P280-P370+P378-P501-P261-P270-P271-P264-P337+P313-P305+P351+P338-P361+P364-P332+P313-P301+P310+P330-P302+P352+P312-P304+P340+P311-P403+P233-P405 | UN#: | 2926 |
Hazard Statements: | H228-H301+H311+H331-H315-H319 | Packing Group: | Ⅱ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With nitric acid |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
1: 16% 2: 18% 3: 53% 4: 60% | With nitric acid In acetic acid at -5℃; for 1h; Further byproducts given; | |
1: 30% 2: 7% 3: 35% 4: 58% | With nitric acid In acetic acid at 20℃; for 1h; Further byproducts given; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
90% | With hydrogenchloride; In methanol; water; | EXAMPLE 2 Preparing 1,3-Dimethgxy-4,6-dinitrobenzene from <strong>[3698-83-7]1,3-Dichloro-4,6-dinitrobenzene</strong> STR6 A 1-liter, 3-necked, round-bottomed flask is charged with 500 mL of methanol, 30 g of crushed potassium hydroxide, 75 mL of water, and 23.7 g (0.10 mole) of 1,3-dichloro-4,6-dinitrobenzene. The reaction mixture is agitated and heated to 65 C. for 8 hours and cooled to 25 C. The reaction mixture is then quenched with an excess of 0 C. aqueous hydrochloric acid. The resulting pale yellow solid is isolated by filtration and air-dried to yield 20 g (90% yield) of 1,3-dimethoxy-4,6-dinitrobenzene, a diether of dinitroresorcinol. |