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[ CAS No. 1214337-82-2 ] {[proInfo.proName]}

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Chemical Structure| 1214337-82-2
Chemical Structure| 1214337-82-2
Structure of 1214337-82-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1214337-82-2 ]

CAS No. :1214337-82-2 MDL No. :MFCD14698341
Formula : C9H10BrNO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 260.09 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 1214337-82-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1214337-82-2 ]

[ 1214337-82-2 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 64-17-5 ]
  • [ 1214334-70-9 ]
  • [ 1214337-82-2 ]
YieldReaction ConditionsOperation in experiment
99% toluene-4-sulfonic acid; for 48h;Reflux; Step 3. Synthesis of ethyl 5-bromo-6-methoxypyridine-2-carboxylate (C16). para-Toluenesulfonic acid hydrate (roughly 0.3 g) was added to a solution of 5- bromo-6-methoxypyridine-2-carboxylic acid (C15) (12.2 g, 52.6 mmol) in ethanol (300 mL). The reaction mixture was heated at reflux for 48 hours, then concentrated in vacuo to provide the title product. Yield: 13.5 g, 51 .9 mmol, 99%.
97% With chloro-trimethyl-silane; at 20℃; for 2h; To a solution of <strong>[1214334-70-9]5-bromo-6-methoxypicolinic acid</strong> (1.03 g, 4.42 mmol) in ethanol (25 mL) trimethylsilyl chloride (3.84 g, 35.3 mmol) was added. The mixture was stirred at rt for 2 h before it was concentrated. The remaining residue was taken up in sat. aq. NaHCO3 solution and extracted three times with EA. The combined organic extracts were dried over MgSO4, filtered and concentrated and dried to give ethyl 5-bromo-6-methoxypicolinate 42 (1.12 g, 97%) as a white solid
  • 2
  • [ 185017-72-5 ]
  • [ 1214337-82-2 ]
  • 3
  • [ 1256823-65-0 ]
  • [ 1214337-82-2 ]
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