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[ CAS No. 1285517-11-4 ]

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2D
Chemical Structure| 1285517-11-4
Chemical Structure| 1285517-11-4
Structure of 1285517-11-4 *Storage: {[proInfo.prStorage]}

Quality Control of [ 1285517-11-4 ]

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Alternatived Products of [ 1285517-11-4 ]
Alternatived Products of [ 1285517-11-4 ]

Product Details of [ 1285517-11-4 ]

CAS No. :1285517-11-4MDL No. :
Formula : C9H14N2O3 Boiling Point : -
Linear Structure Formula :-InChI Key :-
M.W :198.22Pubchem ID :-
Synonyms :

Computed Properties of [ 1285517-11-4 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 1285517-11-4 ]

Signal Word:Class:
Precautionary Statements:UN#:
Hazard Statements:Packing Group:

Application In Synthesis of [ 1285517-11-4 ]

  • Upstream synthesis route of [ 1285517-11-4 ]
  • Downstream synthetic route of [ 1285517-11-4 ]

[ 1285517-11-4 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 1285517-11-4 ]
  • [ 354795-62-3 ]
YieldReaction ConditionsOperation in experiment
93% With trifluoroacetic acid In dichloromethane at 20℃; for 1 h; [0268j A mixture of tert-butyl (3-methylisoxazol-4-yl)carbamate (150 mg, 0.75 mmol) in TFA/DCM (10 mL, 1:1) was stirred at rt for 1 h. After concentrated, the residue was dissolved in DCM (20 mL) and solid K2C03 (1 g) was added. The solid was filtered off and the filtrate was concentrated to give crude title product (96 mg, yield: 93percent), which was used in nest step without further purification.
Reference: [1] Patent: WO2015/89337, 2015, A1, . Location in patent: Paragraph 0268
[2] Patent: WO2011/38572, 2011, A1, . Location in patent: Page/Page column 75
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