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Heterocyclic Building Blocks
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Aryls Bromides

[ CAS No. 13141-26-9 ]

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 13141-26-9
Chemical Structure| 13141-26-9
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SDS Specification
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Product Details of [ 13141-26-9 ]

CAS No. :13141-26-9 MDL No. :
Formula : C14H9BrO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :273.13 Pubchem ID :-
Synonyms :

Safety of [ 13141-26-9 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 13141-26-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13141-26-9 ]

[ 13141-26-9 ] Synthesis Path-Downstream   1~8

  • 1
  • [ 4755-72-0 ]
  • [ 1761-61-1 ]
  • [ 13141-26-9 ]
Reference： [1]Chemische Berichte,1903,vol. 36,p. 3983
  • 2
  • [ 207115-22-8 ]
  • [ 536-74-3 ]
  • [ 13141-26-9 ]
Reference： [1]Organic Letters,2002,vol. 4,p. 4727 - 4729
[2]European Journal of Organic Chemistry,2010,p. 6067 - 6071
  • 3
  • [ 207115-22-8 ]
  • [ 536-74-3 ]
  • [ 13141-26-9 ]
  • [ 1352954-91-6 ]
Reference： [1]Synlett,2011,p. 2590 - 2594
  • 4
  • [ 1719-19-3 ]
  • [ 207115-22-8 ]
  • [ 13141-26-9 ]
Reference： [1]Journal of Chemical Sciences,2011,vol. 123,p. 697 - 702
  • 5
  • [ 10576-12-2 ]
  • [ 139139-81-4 ]
  • [ 98-86-2 ]
  • [ 13141-26-9 ]
  • [ 589-87-7 ]
Reference： [1]Chemistry - A European Journal,2014,vol. 20,p. 8888 - 8892
  • 6
  • [ 116272-41-4 ]
  • [ 13141-26-9 ]
Reference： [1]Organic and Biomolecular Chemistry,2015,vol. 13,p. 2273 - 2284
  • 7
  • [ 23145-07-5 ]
  • [ 109674-45-5 ]
  • [ 13141-26-9 ]
YieldReaction ConditionsOperation in experiment
77% With trifluorormethanesulfonic acid; C24H36N2O2Pd*2C2H4O2; cesium trifluoroacetate; trifluoroacetic acid; p-benzoquinone; silver(l) oxide; In water; at 30℃; for 20h; General procedure: To a 10 mL round-bottom flask were added Cat.III (3.2 mg, 0.005 mmol, 2 mol %), Ag2O (116 mg, 0.5 mmol, 2 equiv), benzoquinone (14 mg, 0.125 mmol, 0.5 equiv), Cs(tfa) (64 mg, 0.25 mmol, 1 equiv.), benzothiophene/benzofurans (0.25 mmol, 1 equiv), aryl MIDA boronate ( 0.375 mmol, 1.5 equiv), and 15% H2O and 2% CF3SO3H of TFA (1 mL). The reaction mixture was stirred at 30-50 C for 20 h. The suspension was cooled to room temperature and extracted with dichloromethane (3 × 10 mL). The combined organic layers were washed with 20% aqueous NaHCO3 solution (40 mL). After evaporation of the solvent the crude product was purified by chromatography on silica gel to give the desired product.
Reference： [1]Synlett,2015,vol. 26,p. 531 - 536
  • 8
  • [ 147034-01-3 ]
  • [ 13141-26-9 ]
Reference： [1]Organic Letters,2018,vol. 20,p. 3310 - 3313

Tags: 13141-26-9 synthesis path| 13141-26-9 SDS| 13141-26-9 COA| 13141-26-9 purity| 13141-26-9 application| 13141-26-9 NMR| 13141-26-9 COA| 13141-26-9 structure

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