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CAS No. : | 135782-64-8 | MDL No. : | |
Formula : | C12H8ClN3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 229.67 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
63% | With Imidazole hydrochloride at 153℃; | General procedure for the synthesis of 1,2,4-triazolo[3,4-a]pyridine derivatives (4a-4g) General procedure: 2-Hydrazinylpyridine (0.5 mmol), imidazolium chloride (0.05 mmol) was added into DMAC/N,N-dimethylbenzamide (2.0 g), and the mixture was stirred at 153 for 3-12 hours till completion as indicated by TLC. DMAC/N,N-dimethylbenzamide was removed by rotary evaporator and the residue was applied to flash column chromatography on silica gel to afford the desired product. |