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[ CAS No. 1369207-07-7 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 1369207-07-7
Chemical Structure| 1369207-07-7
Structure of 1369207-07-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1369207-07-7 ]

CAS No. :1369207-07-7 MDL No. :
Formula : C11H12N2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 172.23 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 1369207-07-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1369207-07-7 ]

[ 1369207-07-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 635-80-3 ]
  • [ 1369207-07-7 ]
  • 2
  • [ 73013-69-1 ]
  • [ 1369207-07-7 ]
YieldReaction ConditionsOperation in experiment
97% With ammonia; hydrogen In methanol at 20℃; for 16h; 13.5 Step 5: (2-methylquinolin-6-yl)methanamine: Step 5: (2-methylquinolin-6-yl)methanamine: To a solution of 2-methylquinoline-6- carbonitrile (0.700 g, 4.16 mmol) in saturated ammonia in methanol (10 ml ), Raney-Ni (1.4g) was added and the mixture was stirred at 1 atm of at RT for 16h. The reaction mixture was filtered and the filtrate was concentrated under vacuum to afford the title compound as a brown oil (0.700 g, 97%). 'H-NMR (δ ppm, DMSO-d6, 400 MHz): 8.83 (dd, J = 4.2, 1.7 Hz, 1H), 8.29 (d, J = 8.3 Hz, 1H), 7.95 (d, J = 8.6 Hz, 1H), 7.85 (s, 1H), 7.75 (dd J = 8.7,1.8 Hz, 1H), 7.49 (dd, J = 8.2,4.2 Hz, 1H), 3.90 (s, 2H).
97% With ammonia; hydrogen In methanol at 20℃; for 16h; 5 Step 5:
(2-methylquinolin-6-yl)methanamine Step 5: (2-methylquinolin-6-yl)methanamine To a solution of 2-methylquinoline-6-carbonitrile (0.700 g, 4.16 mmol) in saturated ammonia in methanol (10 ml), Raney-Ni (1.4 g) was added and the mixture was stirred at 1 atm of H2 at RT for 16 h. The reaction mixture was filtered and the filtrate was concentrated under vacuum to afford the title compound as a brown oil (0.700 g, 97%). 1H-NMR (δ ppm, DMSO-d6, 400 MHz): 8.83 (dd, J=4.2, 1.7 Hz, 1H), 8.29 (d, J=8.3 Hz, 1H), 7.95 (d, J=8.6 Hz, 1H), 7.85 (s, 1H), 7.75 (dd J=8.7, 1.8 Hz, 1H), 7.49 (dd, J=8.2, 4.2 Hz, 1H), 3.90 (s, 2H).
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