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[ CAS No. 13925-00-3 ] {[proInfo.proName]}

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Chemical Structure| 13925-00-3
Chemical Structure| 13925-00-3
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Product Details of [ 13925-00-3 ]

CAS No. :13925-00-3 MDL No. :MFCD00006149
Formula : C6H8N2 Boiling Point : -
Linear Structure Formula :- InChI Key :KVFIJIWMDBAGDP-UHFFFAOYSA-N
M.W : 108.14 Pubchem ID :26331
Synonyms :

Safety of [ 13925-00-3 ]

Signal Word:Danger Class:3
Precautionary Statements:P210-P233-P240-P241-P242-P301+P312 UN#:1993
Hazard Statements:H225-H302 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 13925-00-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 13925-00-3 ]
  • Downstream synthetic route of [ 13925-00-3 ]

[ 13925-00-3 ] Synthesis Path-Upstream   1~30

  • 1
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Reference: [1] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993, vol. 29, # 11, p. 1308 - 1315[2] Khimiya Geterotsiklicheskikh Soedinenii, 1993, # 11, p. 1516 - 1525
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Reference: [1] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993, vol. 29, # 11, p. 1308 - 1315[2] Khimiya Geterotsiklicheskikh Soedinenii, 1993, # 11, p. 1516 - 1525
[3] Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990, vol. 39, # 7.1, p. 1340 - 1345[4] Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990, # 7, p. 1483 - 1488
[5] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993, vol. 29, # 11, p. 1308 - 1315[6] Khimiya Geterotsiklicheskikh Soedinenii, 1993, # 11, p. 1516 - 1525
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Reference: [1] Journal of Organic Chemistry, 1959, vol. 24, p. 691
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Reference: [1] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993, vol. 29, # 11, p. 1308 - 1315[2] Khimiya Geterotsiklicheskikh Soedinenii, 1993, # 11, p. 1516 - 1525
[3] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993, vol. 29, # 11, p. 1308 - 1315[4] Khimiya Geterotsiklicheskikh Soedinenii, 1993, # 11, p. 1516 - 1525
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Reference: [1] Journal of Agricultural and Food Chemistry, 2010, vol. 58, # 4, p. 2470 - 2478
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Reference: [1] Journal of Agricultural and Food Chemistry, 2015, vol. 63, # 22, p. 5364 - 5372
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Reference: [1] Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990, vol. 39, # 7.1, p. 1340 - 1345[2] Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990, # 7, p. 1483 - 1488
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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Reference: [1] Journal of Agricultural and Food Chemistry, 2012, vol. 60, # 18, p. 4697 - 4708
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  • [ 15707-23-0 ]
Reference: [1] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993, vol. 29, # 11, p. 1308 - 1315[2] Khimiya Geterotsiklicheskikh Soedinenii, 1993, # 11, p. 1516 - 1525
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Reference: [1] Journal of Agricultural and Food Chemistry, 1999, vol. 47, # 10, p. 4332 - 4335
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Reference: [1] Journal of Agricultural and Food Chemistry, 2012, vol. 60, # 18, p. 4697 - 4708
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Reference: [1] Journal of Agricultural and Food Chemistry, 2012, vol. 60, # 18, p. 4697 - 4708
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YieldReaction ConditionsOperation in experiment
66 %Spectr. With tert.-butylhydroperoxide In water at 60℃; for 12 h; General procedure: A 15‐mL RBF was charged with substrate (0.5 mmol),MnOx‐N(at)C catalyst (1 mg, pyrolysis at 600 °C) and TBHP (1.5mmol, 65percent in H2O). The flask was then sealed, and the mixturewas heated at 60 °C for 12 h. The reaction was cooled to roomtemperature and diluted with ethyl acetate (4 mL), before beingcentrifuged at 10000 r/min for 1 min to separate the catalyst.The supernatant was removed and the catalyst waswashed with ethyl acetate (5 × 4 mL). The supernatant wassubsequently combined the ethyl acetate wash solutions andevaporated to dryness to give a residue, which was purified byflash column chromatography over silica gel (ethyl acetate/n‐hexane = 1:10, v/v).
Reference: [1] Chinese Journal of Catalysis, 2016, vol. 37, # 8, p. 1216 - 1221
  • 20
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Reference: [1] Journal of Organic Chemistry, 1959, vol. 24, p. 691
[2] Journal of Chemical Thermodynamics, 2005, vol. 37, # 1, p. 49 - 53
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Reference: [1] Journal of Chemical Thermodynamics, 2005, vol. 37, # 1, p. 49 - 53
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Reference: [1] Journal of Chemical Thermodynamics, 2005, vol. 37, # 1, p. 49 - 53
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Reference: [1] Journal of Agricultural and Food Chemistry, 2012, vol. 60, # 18, p. 4697 - 4708
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Reference: [1] Journal of Agricultural and Food Chemistry, 2012, vol. 60, # 18, p. 4697 - 4708
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Reference: [1] Journal of Agricultural and Food Chemistry, 2012, vol. 60, # 18, p. 4697 - 4708
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Reference: [1] Journal of Agricultural and Food Chemistry, 2015, vol. 63, # 22, p. 5364 - 5372
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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Reference: [1] Food Chemistry, 2010, vol. 119, # 1, p. 214 - 219
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  • [ 109-08-0 ]
  • [ 123-32-0 ]
  • [ 13925-00-3 ]
  • [ 693-98-1 ]
  • [ 15707-23-0 ]
Reference: [1] Chemistry of Heterocyclic Compounds (New York, NY, United States), 1993, vol. 29, # 11, p. 1308 - 1315[2] Khimiya Geterotsiklicheskikh Soedinenii, 1993, # 11, p. 1516 - 1525
  • 30
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  • [ 94777-52-3 ]
Reference: [1] Patent: US4638005, 1987, A,
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