Alternatived Products of [ 1453097-62-5 ]
Product Details of [ 1453097-62-5 ]
CAS No. : | 1453097-62-5 |
MDL No. : | MFCD26689254 |
Formula : |
C8H7F3N4
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
216.16
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 1453097-62-5 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 1453097-62-5 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1453097-62-5 ]
- 1
-
[ 86604-86-6 ]
-
[ 1453097-62-5 ]
Yield | Reaction Conditions | Operation in experiment |
|
With hydrazine hydrate; at 100℃; |
General procedure: A mixture of 2-chloro-5-methyl-benzimidazole (10.2 g, 61.2 mmol) and hydrazine monohydrate (59 mL, 1.22 mol) was stirred at 100 C overnight. After being cooled to ambient temperature, to the reaction mixture was added to water (60 mL). After stirring under ice cooling, the resulting precipitates were collected by filtration. The precipitates were washed with water 3 times, and then dried in vacuo to give 2-hydrazino-5-methyl-benzimidazole (8.4 g, 84.6%). |
Categories