Alternatived Products of [ 1644664-02-7 ]
Product Details of [ 1644664-02-7 ]
CAS No. : | 1644664-02-7 |
MDL No. : | MFCD28405539 |
Formula : |
C15H19BClN3O2
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
319.59
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 1644664-02-7 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 1644664-02-7 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 1644664-02-7 ]
- 1
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[ 1114809-11-8 ]
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[ 1644664-02-7 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 2 h / 140 °C
2: tetrabutyl-ammonium chloride; chloro-trimethyl-silane; tert.-butylnitrite / N,N-dimethyl-formamide; dichloromethane / 1 h / 0 - 50 °C
3: ethanol / 1 h / 80 °C / Sealed tube
4: 1,1'-bis(diphenylphosphino)ferrocene-palladium(II)dichloride dichloromethane complex; potassium acetate / 1,4-dioxane / 2.5 h / 110 °C |
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Reference:
[1]Smith, Adrian L.; Andrews, Kristin L.; Beckmann, Holger; Bellon, Steven F.; Beltran, Pedro J.; Booker, Shon; Chen, Hao; Chung, Young-Ah; D'Angelo, Noel D.; Dao, Jennifer; Dellamaggiore, Kenneth R.; Jaeckel, Peter; Kendall, Richard; Labitzke, Katja; Long, Alexander M.; Materna-Reichelt, Silvia; Mitchell, Petia; Norman, Mark H.; Powers, David; Rose, Mark; Shaffer, Paul L.; Wu, Michelle M.; Lipford, J. Russell
[Journal of Medicinal Chemistry, 2015, vol. 58, # 3, p. 1426 - 1441]