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[ CAS No. 1951483-74-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 1951483-74-1
Chemical Structure| 1951483-74-1
Structure of 1951483-74-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1951483-74-1 ]

CAS No. :1951483-74-1 MDL No. :MFCD30530865
Formula : C8H9NOS Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 167.23 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 1951483-74-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1951483-74-1 ]

[ 1951483-74-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1951483-74-1 ]
  • [ 1951483-29-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 5 steps 1: N-Bromosuccinimide / acetonitrile / 6 h / 10 - 25 °C 2: sodium hydroxide; tetra-(n-butyl)ammonium iodide / 1,4-dioxane; water / 1 h / 80 °C 3: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere 4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / 1,4-dioxane; water / 1 h / 90 °C / Inert atmosphere 5: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium diacetate / 1,4-dioxane / 90 °C / Inert atmosphere
Multi-step reaction with 7 steps 1: N-Bromosuccinimide / acetonitrile / 6 h / 10 - 25 °C 2: dmap; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C 3: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 4 h / 90 °C / Inert atmosphere 4: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 2 h / 90 °C / Inert atmosphere 5: trifluoroacetic acid / dichloromethane / 2 h / 20 °C 6: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C 7: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium diacetate / 1,4-dioxane / 90 °C / Inert atmosphere
Multi-step reaction with 4 steps 1.1: N-Bromosuccinimide / acetonitrile / 6 h / 10 - 25 °C 2.1: sodium hydroxide; tetra-(n-butyl)ammonium iodide / 1,4-dioxane; water / 1 h / 80 °C 3.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 1 h / 90 °C 3.2: 1 h / 50 - 90 °C 4.1: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 85 °C
Multi-step reaction with 7 steps 1.1: N-Bromosuccinimide / acetonitrile / 6 h / 10 - 25 °C 2.1: dmap; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C 3.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 4 h / 90 °C 4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 1.5 h / 87 °C 5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C 6.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.17 h 6.2: 0 - 20 °C 7.1: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 85 °C
Multi-step reaction with 8 steps 1.1: N-Bromosuccinimide / acetonitrile / 6 h / 10 - 25 °C 2.1: dmap; N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C 3.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 4 h / 90 °C 4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 1.5 h / 87 °C 5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C 6.1: hydrogenchloride / 1,4-dioxane / 20 - 30 °C 7.1: tetra-(n-butyl)ammonium iodide; sodium hydride / mineral oil; 1-methyl-pyrrolidin-2-one / 0.17 h / 0 °C 7.2: 4 h / Cooling 8.1: caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 85 °C

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