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CAS No. : | 20637-07-4 | MDL No. : | |
Formula : | C17H18O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 254.32 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With toluene-4-sulfonic acid; at 100℃; for 6.0h; | (3) adding 0.03 mmol of p-toluenesulfonic acid and 50 mmol of methanol to 1 mmol of the biphenylbutyric acid,The reaction was heated to 100 C under reflux for 6 hours, and the reaction product was distilled off under reduced pressure (the pressure of the reduced pressure distillation was within 100 mbar and the temperature was 80 C or higher),Purification through a silica gel column (flushing the chromatography silica gel column with petroleum ether over ethyl acetate 1:20) to obtain methyl biphenylbutyrate; |