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[ CAS No. 213136-12-0 ] {[proInfo.proName]}

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Chemical Structure| 213136-12-0
Chemical Structure| 213136-12-0
Structure of 213136-12-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 213136-12-0 ]

CAS No. :213136-12-0 MDL No. :MFCD22666305
Formula : C23H18BrFN2O7 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 533.30 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 213136-12-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 213136-12-0 ]

[ 213136-12-0 ] Synthesis Path-Downstream   1~3

  • 2
  • [ 213136-12-0 ]
  • [ 69123-98-4 ]
YieldReaction ConditionsOperation in experiment
Stage #1: 1-(3',5'-di-O-benzoyl-2'-deoxy-2'-fluoro-β-D-arabinofuranosyl)-5-bromouracil With tris(1H,1H,2H,2H-perfluorooctyl)tin hydride; palladium diacetate; 1,3,5,7-tetramethyl-6-(2,4-dimethoxyphenyl)-2,4,8-trioxa-6-phosphaadamantane In tetrahydrofuran at 65℃; Inert atmosphere; Stage #2: With sodium methylate In tetrahydrofuran; methanol Stage #3: With iodine; acetic acid Further stages;
  • 3
  • C10H23BrN2O2Si2 [ No CAS ]
  • [ 97614-44-3 ]
  • [ 213136-12-0 ]
YieldReaction ConditionsOperation in experiment
at 90℃; for 20h; Inert atmosphere; 3 Example 31-(3,5-di-oxy-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-bromouracil (1-(3,5-di- Synthesis of O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-bromouracil) Take 0.71 g, 1.68 mmoles of 2-deoxy-2-fluoro-3,5-di-oxo-benzamido-α-D-bromoarabinofuranosyl,In the presence of nitrogen,0.71 g, 1.68 mmoles of 2,4-bis-oxo-(trimethylmercapto)-5-bromouracil are added,The mixture was heated under reflux at 90°C and stirred for 20 hours.Next, the solvent remaining in the above reaction is first concentrated under reduced pressure, washed with hexane, and suction filtered.Finally, it is washed with a little diethyl ether and its solid is taken to obtain 1-(3,5-di-oxy-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5- Bromouracil (1-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-bromouracil).
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