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Cytoskeleton
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Cyclo(RGDyK)
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Peptide

[ CAS No. 217099-14-4 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 217099-14-4
Chemical Structure| 217099-14-4
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Quality Control of [ 217099-14-4 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification
Alternatived Products of [ 217099-14-4 ]

Product Details of [ 217099-14-4 ]

CAS No. :217099-14-4 MDL No. :MFCD08459533
Formula : C27H41N9O8 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 619.67 Pubchem ID :-
Synonyms :

Safety of [ 217099-14-4 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 217099-14-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 217099-14-4 ]

[ 217099-14-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ CAS Unavailable ]
  • [ 217099-14-4 ]
  • [ 170908-81-3 ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
50.5% Stage #1: [(2S,5R,8S,11S)-8-(4-Amino-butyl)-11-(3-guanidino-propyl)-5-(4-hydroxy-benzyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaaza-cyclopentadec-2-yl]-acetic acid; 1,4,7,10-tetraazacyclododecane-1,4,7,10-tetraacetic acid mono(N-hydroxysuccinimidyl ester) With O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 20℃; for 4h; Stage #2: lanthanum nitrate In 1-methyl-pyrrolidin-2-one Compound (12): c(RGDyK)-(DOTA-La). Compound (12): c(RGDyK)-(DOTA-La). To a solution of NHS-DOTA (Macrocyclics), (2.0 mg, 3.14×10-3 mmol) dissolved in NMP (1.0 mL), the targeting peptide c(RGDyK) (Peptides, International) (1.95 mg, 3.14×10-3 mmol) in NMP (1.0 mL) with DIPA (4.07 mg, 3.15×10-2 mmol) and TSTU (1.90 mg, 6.30×10-3 mmol) was added. The solution was stirred for 4 h at room temperature while using LC-MS method B: 5-100% to check the reaction progress. Once the reaction was complete, the solid La(NO3)2 (3.41 mg, 7.87 mmol) was added, again following by LC-MS method B: 5-100% to check the reaction progress which was immediate. Diethyl ether (5 mL) was added to precipitate the product which was vortexed and centrifuged in a 15 mL centrifuge tube This product was purified through SPE using method B: 5-50% with product found in fractions 5-20%. Yield: 1.2 mg (1.03×10-3 mmol, 50.5%); LC-MS=Calcd. for C43H64LaN13O15: 1141.37 (m/z). found: 1140.40 [M-H]-; 570 [(M-2H/2]-.
Reference： [1]Current Patent Assignee: ROCHESTER INSTITUTE OF TECHNOLOGY - US2016/251378, 2016, A1 Location in patent: Paragraph 0080

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[ 217099-14-4 ]

Chemical Structure| 250612-42-1

A193345[ 250612-42-1 ]

2,2,2-Trifluoroacetic acid compound with 2-((2S,5R,8S,11S)-8-(4-aminobutyl)-11-(3-guanidinopropyl)-5-(4-hydroxybenzyl)-3,6,9,12,15-pentaoxo-1,4,7,10,13-pentaazacyclopentadecan-2-yl)acetic acid (2:1)

Reason: Free-salt