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[ CAS No. 225122-33-8 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 225122-33-8
Chemical Structure| 225122-33-8
Structure of 225122-33-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 225122-33-8 ]

CAS No. :225122-33-8 MDL No. :MFCD24392169
Formula : C14H23N3O3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 281.35 Pubchem ID :-
Synonyms :

Safety of [ 225122-33-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 225122-33-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 225122-33-8 ]

[ 225122-33-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 6011-14-9 ]
  • [ 115951-16-1 ]
  • [ 225122-33-8 ]
YieldReaction ConditionsOperation in experiment
Boc-1-aminocyclohexane carboxylic acid (40 mmol), HOBt (40 mmol) and WSCD (42 mmol) are dissolved in dimethylformamide (75 ml) and stirred for 15 min. at RT. 2-aminoacetonitrile hydrochloride (40 mmol) and triethylamine (40 mmol) are suspended in DMF (25 ml) and added to the reaction mixture which is stirred at 25 C. over night. After evaporation of the solvent, the residue is extracted with ethyl acetate. The extract is washed with water, 10% citric acid, brine, sodium bicarbonate, brine and dried over magnesium sulfate and evaporated. The residue is suspended in diethylether and the solid filtered of and dried (vacuum). 7.35 g of a white powder with mp. 160-162 C., Rf=0.28 (n-hexane:ethyl acetate=1:1) is obtained.
  • 2
  • [ 151-63-3 ]
  • [ 115951-16-1 ]
  • [ 225122-33-8 ]
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