[ CAS No. 22966-22-9 ] {[proInfo.proName]}

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Quality Control of [ 22966-22-9 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 22966-22-9 ]

SDS Specification

Alternatived Products of [ 22966-22-9 ]

Product Details of [ 22966-22-9 ]

CAS No. :	22966-22-9	MDL No. :
Formula :	C₁₅H₁₁ClO	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	-
M.W :	242.70	Pubchem ID :	-
Synonyms :

Safety of [ 22966-22-9 ]

Signal Word:		Class:
Precautionary Statements:		UN#:
Hazard Statements:		Packing Group:

Application In Synthesis of [ 22966-22-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 22966-22-9 ]

[ 22966-22-9 ] Synthesis Path-Downstream 1~19

1
[ 39008-28-1 ]
[ 22966-22-9 ]
4-(4-chlorophenyl)-2,3,6,7-tetrahydro-7-methyl-8-methylthio-2-phenyl-1H-pyrimido<4,5-b><1,4>diazepin-6-one [ No CAS ]

Reference： [1]Journal of Heterocyclic Chemistry,1994,vol. 31,p. 61 - 64

2
[ 1004-40-6 ]
[ 22966-22-9 ]
[ 150356-87-9 ]

Reference： [1]Phosphorus, Sulfur and Silicon and the Related Elements,2002,vol. 177,p. 45 - 58
[2]Collection of Czechoslovak Chemical Communications,2005,vol. 70,p. 350 - 360

3
[ 22966-22-9 ]
[ 5739-37-7 ]

Yield	Reaction Conditions	Operation in experiment
98%	With hydrogen In methanol for 20h;
98%	With hydrogen In methanol at 20℃; for 20h;
98%	With hydrogen In methanol at 20℃; for 24h;

97%	With diphenyl sulfide; hydrogen In methanol at 20℃; for 24h;
97%	With diphenyl sulfide; hydrogen In methanol at 20℃; for 24h;
96%	With ammonium acetate; zinc In ethanol at 20℃; for 1.25h;
92%	With 9-borabicyclo[3.3.1]nonane dimer; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In ethyl acetate at 40℃; for 16h;
90%	With sodium tetrahydroborate; nickel dichloride In methanol; water at 20℃; for 0.5h;
90%	With ammonium chloride; zinc In ethanol; water at 20℃; for 0.75h;
86%	With magnesium; zinc(II) chloride for 0.416667h;
	Multi-step reaction with 2 steps 1: sodium tetrahydroborate; cerium(III) chloride monohydrate / methanol / 0.17 h 2: sodium t-butanolate; 1,10-Phenanthroline / toluene / 2 h / 80 °C / Inert atmosphere

Reference： [1]Sajiki, Hironao; Ikawa, Takashi; Yamada, Hiromi; Tsubouchi, Kozo; Hirota, Kosaku [Tetrahedron Letters, 2003, vol. 44, # 1, p. 171 - 174]
[2]Ikawa, Takashi; Sajiki, Hironao; Hirota, Kosaku [Tetrahedron, 2005, vol. 61, # 8, p. 2217 - 2231]
[3]Kitamura, Yoshiaki; Tanaka, Asami; Sato, Mutsumi; Oono, Keiji; Ikawa, Takashi; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao [Synthetic Communications, 2007, vol. 37, # 24, p. 4381 - 4388]
[4]Mori, Akinori; Miyakawa, Yumi; Ohashi, Eri; Haga, Tomoko; Maegawa, Tomohiro; Sajiki, Hironao [Organic Letters, 2006, vol. 8, # 15, p. 3279 - 3281]
[5]Mori, Akinori; Mizusaki, Tomoteru; Miyakawa, Yumi; Ohashi, Eri; Haga, Tomoko; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao [Tetrahedron, 2006, vol. 62, # 51, p. 11925 - 11932]
[6]Zhou, Yong-Bo; Wang, Yu-Iu; Wang, Jin-Ye [Journal of Chemical Research, 2004, # 2, p. 118 - 119]
[7]Nicholson, Kieran; Langer, Thomas; Thomas, Stephen P. [Organic Letters, 2021, vol. 23, # 7, p. 2498 - 2504]
[8]Khurana, Jitender Mohan; Sharma, Purnima [Bulletin of the Chemical Society of Japan, 2004, vol. 77, # 3, p. 549 - 552]
[9]Li, Jian-Ping; Zhang, Yong-Xia; Ji, Yan [Journal of the Chinese Chemical Society, 2008, vol. 55, # 2, p. 390 - 393]
[10]Saikia, Anil; Barthakur, Madan Gopal; Boruah, Romesh Chandra [Synlett, 2005, # 3, p. 523 - 525]
[11]Zheng, Hong-Xing; Xiao, Zu-Feng; Yao, Chuan-Zhi; Li, Qiang-Qiang; Ning, Xiao-Shan; Kang, Yan-Biao; Tang, Yong [Organic Letters, 2015, vol. 17, # 24, p. 6102 - 6105]

4
[ 1004-40-6 ]
[ 22966-22-9 ]
[ 150356-90-4 ]

Reference： [1]Collection of Czechoslovak Chemical Communications,2005,vol. 70,p. 350 - 360

5
[ 63636-89-5 ]
[ 22966-22-9 ]
(E)-1-(4-chlorophenyl)-3-phenyl-N-[(2-pyridyl)sulfonyl]prop-2-en-1-imine [ No CAS ]

Reference： [1]Journal of Organic Chemistry,2005,vol. 70,p. 7451 - 7454

6
[ 112-44-7 ]
[ 22966-22-9 ]
1-(4-chlorophenyl)-3-phenyltetradecane-1,4-dione [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
97%	With triethylamine In N,N-dimethyl-formamide at 80℃; for 22h;

Reference： [1]Barrett, Anthony G. M.; Love, Andrew C.; Tedeschi, Livio [Organic Letters, 2004, vol. 6, # 19, p. 3377 - 3380]

7
[ 35203-91-9 ]
[ 22966-22-9 ]
(E)-1-(4-chlorophenyl)-3-phenyl-N-[(8-quinoyl)sulfonyl]prop-2-en-1-imine [ No CAS ]

Reference： [1]Journal of the American Chemical Society,2007,vol. 129,p. 1480 - 1481

8
[ 7677-24-9 ]
[ 22966-22-9 ]
[ 6273-45-6 ]

Yield	Reaction Conditions	Operation in experiment
72%	Stage #1: trimethylsilyl cyanide; (E)-1-(4-chlorophenyl)-3-phenyl-2-propen-1-one for 0.0833333h; microwave irradiation; Stage #2: With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 0.0833333h;

Reference： [1]Iida, Hirokazu; Moromizato, Tatsuya; Hamana, Hiroshi; Matsumoto, Kiyoshi [Tetrahedron Letters, 2007, vol. 48, # 11, p. 2037 - 2039]

9
[ 70591-20-7 ]
[ 22966-22-9 ]
C₃₀H₂₃ClN₂O [ No CAS ]

Reference： [1]Synthetic Communications,2007,vol. 37,p. 3971 - 3979

10
[ 98-54-4 ]
[ 22966-22-9 ]
6-tert-butyl-2-(4-chlorophenyl)-4-phenyl-2H-chromen-2-ol [ No CAS ]
[ 5739-37-7 ]

Yield	Reaction Conditions	Operation in experiment
1: 69% 2: 68%	With trifluoroacetic acid for 72h; Heating;

Reference： [1]Wu, Yan-Chao; Liu, Li; Liu, Yu-Liang; Wang, Dong; Chen, Yong-Jun [Journal of Organic Chemistry, 2007, vol. 72, # 24, p. 9383 - 9386]

11
[ 22966-22-9 ]
[ 5034-06-0 ]
C₁₆H₁₃ClO [ No CAS ]
[ 959936-89-1 ]

Reference： [1]Journal of the American Chemical Society,2007,vol. 129,p. 13410 - 13411

12
[ 1117-19-7 ]
[ 22966-22-9 ]
[ 1012919-08-2 ]

Yield	Reaction Conditions	Operation in experiment
98%	With 4 A molecular sieve In toluene at 25℃; for 7h;

Reference： [1]Agostinho, Magno; Kobayashi, Shu [Journal of the American Chemical Society, 2008, vol. 130, # 8, p. 2430 - 2431]

13
[ 140-10-3 ]
[ 7099-88-9 ]
[ 22966-22-9 ]

Reference： [1]Journal of Organic Chemistry,2015,vol. 80,p. 3586 - 3596

14
[ 591-50-4 ]
[ 3946-29-0 ]
[ 22966-22-9 ]

Yield	Reaction Conditions	Operation in experiment
86%	With palladium diacetate; potassium carbonate; triphenylphosphine In N,N-dimethyl-formamide at 20 - 90℃; for 16h; Inert atmosphere;	General procedure for the synthesis of chalcones - synthesis of chalcone 3a General procedure: A mixture of Pd(OAc)2 (4.5 mg, 0.02 mmol), PPh3 (11.2 mg, 0.04 mmol), iodobenzene (1a) (82 mg, 0.4mmol), 3-chloropropiophenone (2a) (87 mg, 0.5 mmol), and K2CO3 (166 mg, 1.2 mmol) in DMF (2.5 mL) was stirred under a N2 atmosphere at room temperature for 10 min, and then heated at 90 °C for 16 h. The reaction was then cooled to ambient temperature and diluted with CH2Cl2 (10 mL) before being filtered through a short pad of silica gel. The silica pad was rinsed with DCM (5 mL), and the combined filtrates were washed with brine (15 mL), dried over anhydrous Na2SO4. The solvent was then removed under reduced pressure to give the crude product as a residue, which was purified by silica gel column chromatography eluting with a mixture of petroleum ether (60-90 °C)/EtOAc (v/v = 30:1).

Reference： [1]Guo, Tenglong; Jiang, Quanbin; Yu, Likun; Yu, Zhengkun [Chinese Journal of Catalysis, 2015, vol. 36, # 1, p. 78 - 85]

15
[ 22966-22-9 ]
[ 67-68-5 ]
[ 116941-51-6 ]

Yield	Reaction Conditions	Operation in experiment
51%	With sodium t-butanolate at 60℃; for 5h;	5 Preparation of 1- (4-chlorophenyl) -3,5-diphenylbenzene mmol of 4'-chlorchalcone, 1.5 mmol of t-butoxide and 2.0 mL of dimethylsulfoxide were added to 10 mL ofShould be placed in the oil bath at 60 , the exposure in the air reaction 5h. The reaction was stopped and allowed to cool to room temperature. The reaction solution is usedDiluted with ethyl acetate and extracted three times with water. The organic phase was dried over anhydrous Na2SO4, filtered and chromatographed to give 20.6Mg of the target product in a yield of 51%.

Reference： [1]Current Patent Assignee: HUAQIAO UNIVERSITY - CN105037072, 2016, B Location in patent: Paragraph 0033; 0034; 0035

16
[ 22966-22-9 ]
[ 111836-35-2 ]
(S)-methyl 2-((R)-3-(4-chlorophenyl)-3-oxo-1-phenylpropyl)-5-phenyl-3,4-dihydro-2H-pyrrole-2-carboxylate [ No CAS ]
C₂₇H₂₄ClNO₃ [ No CAS ]

Reference： [1]Journal of Organic Chemistry,2017,vol. 82,p. 8927 - 8932

17
[ 22966-22-9 ]
[ 111836-35-2 ]
C₂₇H₂₄ClNO₃ [ No CAS ]

Reference： [1]Journal of Organic Chemistry,2017,vol. 82,p. 8927 - 8932

18
[ 22966-22-9 ]
[ 6752-16-5 ]
2-(4-chlorophenyl)-4-phenylpyrido[2’,3’:3,4]pyrazolo[1,5-a]pyrimidine [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
90%	With cholin hydroxide; In neat (no solvent); at 80℃; for 0.833333h;Green chemistry;	General procedure: ChOH (1 mmol) was added to a mixture of <strong>[6752-16-5]1H-pyrazolo[3,4-b]pyridin-3-amine</strong> (1,1.0 mmol) and (2E)-1,3-diphenylprop-2-en-1-one (2a, 1.0 mmol) in a 10-mL reaction flask equipped with a magnetic stirrer. The resulting mixture was stirred for the appropriate time at 80 C. After completion of the reaction (confirmed by TLC, hexane:EtOAc 1:1), 2 mL of water was added and stirred 60 for minutes at room temperature. The solid product was filtered and washed with water. The obtained crude product was recrystallized from ethanol to yield the pure product 3a. The same method was adopted for the synthesis of all the targeted products 3a-3aj.

Reference： [1]Research on Chemical Intermediates,2018,vol. 44,p. 7311 - 7329

19
[ 5739-37-7 ]
[ 22966-22-9 ]

Yield	Reaction Conditions	Operation in experiment
98%	With iron(III) chloride; 1,10-Phenanthroline; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In dimethyl sulfoxide at 120℃; for 24h; Inert atmosphere; Schlenk technique;

Reference： [1]Zhang, Xiao-Wei; Jiang, Guo-Qing; Lei, Shu-Hui; Shan, Xiang-Huan; Qu, Jian-Ping; Kang, Yan-Biao [Organic Letters, 2021, vol. 23, # 5, p. 1611 - 1615]

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P321
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P342	If experiencing respiratory symptoms:
P350	Gently wash with plenty of soap and water.
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P352	Wash with plenty of soap and water.
P353	Rinse skin with water/shower.
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P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
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H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 22966-22-9 ] {[proInfo.proName]}

Quality Control of [ 22966-22-9 ]

Related Doc. of [ 22966-22-9 ]

Product Details of [ 22966-22-9 ]

Safety of [ 22966-22-9 ]

Application In Synthesis of [ 22966-22-9 ]

[ 22966-22-9 ] Synthesis Path-Downstream 1~19

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

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