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[ CAS No. 234098-35-2 ] {[proInfo.proName]}

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Chemical Structure| 234098-35-2
Chemical Structure| 234098-35-2
Structure of 234098-35-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 234098-35-2 ]

CAS No. :234098-35-2 MDL No. :MFCD08689598
Formula : C9H6BrClN2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 257.51 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 234098-35-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 234098-35-2 ]

[ 234098-35-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 90272-83-6 ]
  • [ 234098-35-2 ]
YieldReaction ConditionsOperation in experiment
With N-Bromosuccinimide;dibenzoyl peroxide; In tetrachloromethane; for 8.0h;Heating / reflux; C. 7-Bromomethyl-4-chloroquinazoline. To a solution of <strong>[90272-83-6]4-chloro-7-methylquinazoline</strong> (7.0 g, 39 mmol) in carbon tetrachloride (140 ML) is added N-bromosuccinimide (8.0 g, 45 mmol), and benzoyl peroxide (0.8 g, 3.3 mmol).The solution is refluxed for 8 hours.After this time, the solution is filtered.The filtrate is concentrated and the residue is stirred with ether to give the title compound as an off-white solid (5.1 g, 20 mmol).1H NMR (CDCl3, 300 MHz) delta9.10 (s, 1H), 8.30 (d, 1H), 8.10 (s, 1H), 7.82 (d, 1H), 4.68 (s, 2H). MS (EI): m/z 237 (M+).
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