Alternatived Products of [ 234098-35-2 ]
Product Details of [ 234098-35-2 ]
CAS No. : | 234098-35-2 |
MDL No. : | MFCD08689598 |
Formula : |
C9H6BrClN2
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
257.51
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 234098-35-2 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 234098-35-2 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 234098-35-2 ]
- 1
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[ 90272-83-6 ]
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[ 234098-35-2 ]
Yield | Reaction Conditions | Operation in experiment |
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With N-Bromosuccinimide;dibenzoyl peroxide; In tetrachloromethane; for 8.0h;Heating / reflux; |
C. 7-Bromomethyl-4-chloroquinazoline. To a solution of <strong>[90272-83-6]4-chloro-7-methylquinazoline</strong> (7.0 g, 39 mmol) in carbon tetrachloride (140 ML) is added N-bromosuccinimide (8.0 g, 45 mmol), and benzoyl peroxide (0.8 g, 3.3 mmol).The solution is refluxed for 8 hours.After this time, the solution is filtered.The filtrate is concentrated and the residue is stirred with ether to give the title compound as an off-white solid (5.1 g, 20 mmol).1H NMR (CDCl3, 300 MHz) delta9.10 (s, 1H), 8.30 (d, 1H), 8.10 (s, 1H), 7.82 (d, 1H), 4.68 (s, 2H). MS (EI): m/z 237 (M+). |