Home Cart 0 Sign in  

[ CAS No. 260973-04-4 ]

{[proInfo.proName]}
Cat. No.: {[proInfo.prAm]}
2D
Chemical Structure| 260973-04-4
Chemical Structure| 260973-04-4
Structure of 260973-04-4 *Storage: {[proInfo.prStorage]}

Quality Control of [ 260973-04-4 ]

Purity: {[proInfo.showProBatch.pb_purity]}

Related Doc. of [ 260973-04-4 ]

SDS

Product Details of [ 260973-04-4 ]

CAS No. :260973-04-4MDL No. :MFCD12026047
Formula : C11H7BrF3N Boiling Point : -
Linear Structure Formula :-InChI Key :-
M.W :290.08Pubchem ID :-
Synonyms :

Computed Properties of [ 260973-04-4 ]

TPSA : - H-Bond Acceptor Count : -
XLogP3 : - H-Bond Donor Count : -
SP3 : - Rotatable Bond Count : -

Safety of [ 260973-04-4 ]

Signal Word:WarningClassN/A
Precautionary Statements:P280-P305+P351+P338UN#:N/A
Hazard Statements:H302Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 260973-04-4 ]

  • Downstream synthetic route of [ 260973-04-4 ]

[ 260973-04-4 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 260973-04-4 ]
  • [ 124898-13-1 ]
  • C13H7F8N [ No CAS ]
YieldReaction ConditionsOperation in experiment
<strong>[260973-04-4]4-Bromo-8-methyl-2-trifluoromethylquinoline</strong> Isolated as a waxy white solid, (3.68 g, 72%): IR numax (Nujol)/cm-1 2925, 1467, 1337, 1146, 1113 and 764; NMR deltaH (400 MHz, CDCl3), 2.82 (3H, s), 7.60-7.69 (2H, m), 7.99 (1H, s) and 8.08 (1H, d, J 7.5 Hz).
  • 3
  • [ 260973-04-4 ]
  • [ 736147-23-2 ]
YieldReaction ConditionsOperation in experiment
76% With sodium N-propyldithiocarbamate; In dimethyl sulfoxide; at 35.0℃; for 13.0h; EXAMPLE 3 bis(2-trifluoromethyl-8methyl quinolyl) disulphide To a solution of <strong>[260973-04-4]2-trifluoromethyl-8-methyl-4-bromoquinoline</strong> (0.1 mol) in dimethyl sulphoxide (300 ml), is added sodium salt of propyl dithiocarbamic acid (0.15 mol) in portions.. The stirring continued at 35 C. for 13 hrs and solvent removed under vacuum.. The residue extracted with a mixture of toluene:hexane (60:40), the removal of solvent gives disulphide yield 76%.
76% With sodium N-propyldithiocarbamate; In dimethyl sulfoxide; at 35.0℃; for 13.0h; To a solution of <strong>[260973-04-4]2-trifluoromethyl-8-methyl-4-bromoquinoline</strong> (0.1 mol) in dimethyl sulphoxide (300ml), is added sodium salt of propyl dithiocarbamic acid (0.15 mol) in portions. The stirring continued at 35C for 13 hrs and solvent removed under vacuum. The residue extracted with a mixture of toluene: hexane (60: 40), the removal of solvent gives disulphide yield 76%.
Historical Records