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[ CAS No. 321155-39-9 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 321155-39-9
Chemical Structure| 321155-39-9
Structure of 321155-39-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 321155-39-9 ]

CAS No. :321155-39-9 MDL No. :MFCD06797092
Formula : C9H13NSi Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 163.29 Pubchem ID :-
Synonyms :

Safety of [ 321155-39-9 ]

Signal Word:Danger Class:3
Precautionary Statements:P261-P305+P351+P338 UN#:1993
Hazard Statements:H225-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 321155-39-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 321155-39-9 ]

[ 321155-39-9 ] Synthesis Path-Downstream   1~18

  • 1
  • [ 3437-95-4 ]
  • [ 321155-39-9 ]
  • [ 321155-45-7 ]
YieldReaction ConditionsOperation in experiment
92% With trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 50℃;
92% With trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 50℃; for 24h;
  • 2
  • [ 3437-95-4 ]
  • [ 10486-61-0 ]
  • [ 321155-39-9 ]
  • (Z)-1-dimethyl(2-pyridyl)silyl-2-(2-thianyl)-2-(3-thienyl)ethene [ No CAS ]
YieldReaction ConditionsOperation in experiment
69% Stage #1: 2-Iodothiophene; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: 3-thienyl iodide In tetrahydrofuran at 60℃; for 42h; Further stages.;
  • 3
  • [ 3437-95-4 ]
  • [ 10486-61-0 ]
  • [ 321155-39-9 ]
  • (E)-1-dimethyl(2-pyridyl)silyl-2-(2-thienyl)-2-(3-thienyl)ethene [ No CAS ]
YieldReaction ConditionsOperation in experiment
65% Stage #1: 3-thienyl iodide; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: 2-Iodothiophene In tetrahydrofuran at 60℃; for 42h; Further stages.;
  • 4
  • [ 10486-61-0 ]
  • [ 591-50-4 ]
  • [ 321155-39-9 ]
  • (E)-1-dimethyl(2-pyridyl)silyl-2-phenyl-2-(3-thienyl)ethene [ No CAS ]
YieldReaction ConditionsOperation in experiment
67% Stage #1: iodobenzene; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: 3-thienyl iodide In tetrahydrofuran at 60℃; for 42h; Further stages.;
  • 5
  • [ 10486-61-0 ]
  • [ 591-50-4 ]
  • [ 321155-39-9 ]
  • (Z)-1-dimethyl(2-pyridyl)silyl-2-phenyl-2-(3-thienyl)ethene [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% Stage #1: 3-thienyl iodide; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: iodobenzene In tetrahydrofuran at 60℃; for 42h; Further stages.;
  • 6
  • [ 10486-61-0 ]
  • [ 321155-39-9 ]
  • 2-[Dimethyl-((E)-2-thiophen-3-yl-vinyl)-silanyl]-pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% With trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 50℃;
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃;
  • 7
  • [ 10486-61-0 ]
  • [ 321155-39-9 ]
  • 1-dimethyl(2-pyridyl)silyl-2,2-bis(3-thienyl)ethene [ No CAS ]
YieldReaction ConditionsOperation in experiment
72% With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 9h;
  • 8
  • [ 673-32-5 ]
  • [ 201230-82-2 ]
  • [ 321155-39-9 ]
  • [ 50397-92-7 ]
YieldReaction ConditionsOperation in experiment
75% With dodecacarbonyl-triangulo-triruthenium In toluene at 100℃;
75% Stage #1: carbon monoxide; dimethyl(2-pyridinyl)(vinyl)silane With dodecacarbonyl-triangulo-triruthenium In toluene at 100℃; for 0.166667h; Stage #2: 1-Phenylprop-1-yne In toluene at 100℃; for 24h;
  • 9
  • [ 13041-70-8 ]
  • [ 321155-39-9 ]
  • 2-(Dimethyl-{(E)-2-[4-((E)-styryl)-phenyl]-vinyl}-silanyl)-pyridine [ No CAS ]
YieldReaction ConditionsOperation in experiment
77% With triethylamine In 1,4-dioxane at 20℃;
  • 10
  • [ 109-04-6 ]
  • [ 1719-58-0 ]
  • [ 321155-39-9 ]
  • 11
  • [ 124-38-9 ]
  • [ 321155-39-9 ]
  • [ 74-88-4 ]
  • [ 2459-07-6 ]
YieldReaction ConditionsOperation in experiment
86% With chloro[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene]copper (I); cesium fluoride In tetrahydrofuran at 20℃; for 20h;
> 99 %Spectr. With tetrabutylammonium triphenyldifluorosilicate In tetrahydrofuran-d8 at 25 - 70℃; for 18h; Inert atmosphere; Schlenk technique;
  • 12
  • [ 6952-59-6 ]
  • [ 312693-24-6 ]
  • [ 321155-39-9 ]
  • C23H24N2Si [ No CAS ]
YieldReaction ConditionsOperation in experiment
53% With nickel dibromide In 1-methyl-pyrrolidin-2-one at 20℃; for 48h; regioselective reaction;
  • 13
  • [ 6952-59-6 ]
  • [ 321155-39-9 ]
  • [ 300825-30-3 ]
  • C23H24N2OSi [ No CAS ]
YieldReaction ConditionsOperation in experiment
52% With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction;
  • 14
  • [ 619-42-1 ]
  • [ 321155-39-9 ]
  • [ 300825-30-3 ]
  • C24H27NO3Si [ No CAS ]
YieldReaction ConditionsOperation in experiment
63% With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction;
  • 15
  • [ 106-38-7 ]
  • [ 321155-39-9 ]
  • [ 300825-30-3 ]
  • C23H27NOSi [ No CAS ]
YieldReaction ConditionsOperation in experiment
60% With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction;
  • 16
  • [ 104-92-7 ]
  • [ 312693-24-6 ]
  • [ 321155-39-9 ]
  • C23H27NOSi [ No CAS ]
YieldReaction ConditionsOperation in experiment
50% With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction;
  • 17
  • [ 4387-36-4 ]
  • [ 312693-24-6 ]
  • [ 321155-39-9 ]
  • C23H24N2Si [ No CAS ]
YieldReaction ConditionsOperation in experiment
51% With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction;
  • 18
  • [ 99-90-1 ]
  • [ 254454-47-2 ]
  • [ 321155-39-9 ]
  • [ 2183504-37-0 ]
YieldReaction ConditionsOperation in experiment
44% With nickel dibromide In 1-methyl-pyrrolidin-2-one at 60℃; for 24h; regioselective reaction;
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