There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
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CAS No. : | 321155-39-9 | MDL No. : | MFCD06797092 |
Formula : | C9H13NSi | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 163.29 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Danger | Class: | 3 |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | 1993 |
Hazard Statements: | H225-H315-H319-H335 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
92% | With trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 50℃; | |
92% | With trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 50℃; for 24h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
69% | Stage #1: 2-Iodothiophene; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: 3-thienyl iodide In tetrahydrofuran at 60℃; for 42h; Further stages.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
65% | Stage #1: 3-thienyl iodide; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: 2-Iodothiophene In tetrahydrofuran at 60℃; for 42h; Further stages.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
67% | Stage #1: iodobenzene; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: 3-thienyl iodide In tetrahydrofuran at 60℃; for 42h; Further stages.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | Stage #1: 3-thienyl iodide; dimethyl(2-pyridinyl)(vinyl)silane With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 5h; Stage #2: iodobenzene In tetrahydrofuran at 60℃; for 42h; Further stages.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | With trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 50℃; | |
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; trifuran-2-yl-phosphane; triethylamine In tetrahydrofuran at 60℃; for 9h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | With dodecacarbonyl-triangulo-triruthenium In toluene at 100℃; | |
75% | Stage #1: carbon monoxide; dimethyl(2-pyridinyl)(vinyl)silane With dodecacarbonyl-triangulo-triruthenium In toluene at 100℃; for 0.166667h; Stage #2: 1-Phenylprop-1-yne In toluene at 100℃; for 24h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
77% | With triethylamine In 1,4-dioxane at 20℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
86% | With chloro[1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene]copper (I); cesium fluoride In tetrahydrofuran at 20℃; for 20h; | |
> 99 %Spectr. | With tetrabutylammonium triphenyldifluorosilicate In tetrahydrofuran-d8 at 25 - 70℃; for 18h; Inert atmosphere; Schlenk technique; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
53% | With nickel dibromide In 1-methyl-pyrrolidin-2-one at 20℃; for 48h; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
52% | With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
63% | With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
60% | With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
50% | With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
51% | With nickel dibromide In 1-methyl-pyrrolidin-2-one at 50℃; for 24h; regioselective reaction; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
44% | With nickel dibromide In 1-methyl-pyrrolidin-2-one at 60℃; for 24h; regioselective reaction; |