Alternatived Products of [ 328062-38-0 ]
Product Details of [ 328062-38-0 ]
CAS No. : | 328062-38-0 |
MDL No. : | MFCD09703303 |
Formula : |
C9H14N2O3S
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
230.28
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 328062-38-0 ]
Application In Synthesis of [ 328062-38-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 328062-38-0 ]
- 1
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[ 98-62-4 ]
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[ 109-85-3 ]
-
[ 328062-38-0 ]
Yield | Reaction Conditions | Operation in experiment |
65% |
With triethylamine; In butan-1-ol; for 18h;Heating / reflux; |
Method 24 4-[N-(2-Methoxyethyl)sulphamoyl]aniline A mixture of 2-methoxyethylamine (859mg, 11.4mmol), sulphanilyl fluoride (1.0g, 5.71mmol), and triethylamine (1.72g, 22.9mmol) in n-butanol (15ml) was heated at reflux for 18 hours. The mixture was allowed to cool and the volatiles were removed by evaporation. The residue was purified by chromatography eluding with ethyl acetate / hexane (50:50) increasing in polarity to (70:30) to give the title compound (860mg, 65%). NMR: 2.78 (q, 2H), 3.15 (s, 3H), 3.25 (t, 2H), 5.87 (s, 2H), 6.58 (d, 2H), 7.10 (t, 1H), 7.40 (d, 2H); m/z: 231 [MH]+. |