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CAS No. : | 37994-11-9 | MDL No. : | |
Formula : | C11H9NO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 171.20 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In acetonitrile; at 20℃; | General procedure: Toa solution of the compounds 13a-c, K2CO3(5 equiv) and TBAHS (0.5 equiv) in dry MeCN (20 mL), 1,2,4,5-Tetrakis(bromomethyl)benzene11 (1.2 equiv) was addedand stirred the reaction mixture at rt for 12-24 h. At the conclusion ofreaction (TLC monitoring), excess amount of K2CO3 wasfiltered through the sintered glass funnel and the aqueous layer was extractedwith CH2Cl2. The solvent was removed under reducedpressure and the crude products 14a-cwere directly subjected to next step without further purification. |