Alternatived Products of [ 39946-25-3 ]
Product Details of [ 39946-25-3 ]
CAS No. : | 39946-25-3 |
MDL No. : | MFCD00069752 |
Formula : |
C6H12KNO4S
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
233.33
|
Pubchem ID : | - |
Synonyms : |
2-Morpholinoethanesulphonic acid potassium
|
Application In Synthesis of [ 39946-25-3 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 39946-25-3 ]
- 1
-
[ 39946-25-3 ]
-
β,γ-bidentate Rh(H2O)4ATP
[ No CAS ]
-
P1,P2-bidentate Rh(H2O)4PP
[ No CAS ]
Yield | Reaction Conditions | Operation in experiment |
|
With nucleotide pyrophosphatase byproducts: AMP; pH 5.9, 2 h incubation period at 25°C; reaction mixture was made 1 mM in EDTA and analysed by (31)P-NMR; |
|
- 2
-
C7H15NO4S
[ No CAS ]
-
[ 39946-25-3 ]
Yield | Reaction Conditions | Operation in experiment |
|
With potassium hydroxide In 1,4-dioxane at 80℃; for 15h; |
7.2-7.3 Preparation step S2:
Under stirring conditions, the above 100g compound 3 was added to a 1L dry reactor, the reaction solvent was dioxane, and the M-containing reagent; wherein, the M-containing reagent was potassium hydroxide; the molar ratio of the compound 3 to the M-containing reagent was: 1:1.5, the reaction temperature is 80°C, the reaction pressure is 0.2MPa (gauge pressure), and the reaction time is 15h. After the reaction was completed, the temperature was lowered to normal temperature, and the solvent was removed by rotary evaporation of the reaction solution under reduced pressure and concentrated to obtain a crude product of 2-morpholinoethanesulfonic acid potassium salt with a yield of 76%. Under dry conditions and using a dry closed device, the crude product of 2-morpholinoethanesulfonic acid potassium salt obtained in the preparation step S2 was dissolved in the purification solvent diethyl carbonate, recrystallized, crystallized under low temperature conditions, filtered and dried, A fine product was obtained; the purity of the 2-morpholinoethanesulfonic acid potassium salt product was 99.5%. |