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[ CAS No. 50274-95-8 ] {[proInfo.proName]}

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Chemical Structure| 50274-95-8
Chemical Structure| 50274-95-8
Structure of 50274-95-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 50274-95-8 ]

CAS No. :50274-95-8 MDL No. :MFCD12025222
Formula : C7H5Cl2NO2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 206.03 Pubchem ID :-
Synonyms :

Safety of [ 50274-95-8 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3261
Hazard Statements:H302-H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 50274-95-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 50274-95-8 ]

[ 50274-95-8 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 52301-88-9 ]
  • [ 50274-95-8 ]
YieldReaction ConditionsOperation in experiment
98% With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; for 2h;Heating / reflux; (2-Chloro-4-nitrophenyl)methanol (19 g, 101 mmol) is stirred in a mixture of anhydrous DCM (400 mL), thionyl chloride (15 mL) and DMF (1 mL) for 2 h at boiling temperature. The reaction mixture is evaporated down, the residue is taken up in EtOAc (250 mL), washed with water (5 x 150 mL) and saturated saline solution (150 mL), dried, filtered and evaporated down. Yield: 20.40 g (98%)
With thionyl chloride;N,N-dimethyl-formamide; In dichloromethane; for 2h;Heating / reflux; Method T - 2-chloro-l-chloromethyl-4-nitrobenzene<strong>[52301-88-9](2-chloro-4-nitrophenyl)methanol</strong> (19 g, 101 mmol) is stirred in a mixture of anhydrous dichloromethane (400 mL), thionyl chloride (15 mL) and DMF (1 mL) for 2 h at boiling temperature. The reaction mixture is evaporated down, the residue is taken up in EtOAc (250 mL), washed with water (5 x 150 mL) and saturated saline solution (150 mL), dried on sodium sulphate, filtered and evaporated down. Yield: 20.4 g
  • 2
  • [ 50274-95-8 ]
  • [ 28163-00-0 ]
YieldReaction ConditionsOperation in experiment
80% With ammonium hydroxide; trans-3,5-dihydroperoxy-3,5-dimethyl-1,2-dioxolane; ammonium bromide at 20℃; for 2h; Green chemistry;
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