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[ CAS No. 51385-93-4 ] {[proInfo.proName]}

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Chemical Structure| 51385-93-4
Chemical Structure| 51385-93-4
Structure of 51385-93-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 51385-93-4 ]

CAS No. :51385-93-4 MDL No. :MFCD00453091
Formula : C13H12O3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 216.23 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 51385-93-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 51385-93-4 ]

[ 51385-93-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 51385-93-4 ]
  • [ 17953-58-1 ]
YieldReaction ConditionsOperation in experiment
With water; silver(l) oxide
  • 2
  • [ 1535-67-7 ]
  • [ 3469-26-9 ]
  • [ 51385-93-4 ]
YieldReaction ConditionsOperation in experiment
97% General procedure: In a round-bottomed flask equipped with a stirring bar and rubber septum was placed a 1 M solution of SnCl4 in anhydrous CH2Cl2 (1 mL, 1 mmol). To this solution was added PhSCF2H (1; 240.2 mg, 1.5 mmol) in anhydrous CH2Cl2 (1.5 mL), followed by a solution of an aromatic compound (0.5 mmol) in anhydrous CH2Cl2 (1 mL). The reaction was allowed to proceed for 2 h before it was quenched with a solution of IBX (140 mg, 0.5 mmol) in DMSO/H2O (4 mL; 3:1 v:v). After 2 h of stirring at rt, the reaction mixture was quenched by addition of a saturated aqueous solution of sodium thiosulfate (10 mL), then basified with a saturated aqueous solution of sodium hydrogen carbonate (10 mL), followed by stirring and extraction with CH2Cl2 (3 × 10 mL). The combined organic layers were washed with water (3 × 10 mL) and brine (10 mL), dried (anhydrous MgSO4), filtered and concentrated (aspirator). The residue was purified by PTLC, radial chromatography or column chromatography to furnish analytically pure product.
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