Alternatived Products of [ 5210-99-1 ]
Product Details of [ 5210-99-1 ]
CAS No. : | 5210-99-1 |
MDL No. : | MFCD21987076 |
Formula : |
C9H10ClNO3
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
215.63
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 5210-99-1 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 5210-99-1 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 5210-99-1 ]
- 1
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[ 26455-31-2 ]
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[ 5210-99-1 ]
Yield | Reaction Conditions | Operation in experiment |
76% |
With N-chloro-succinimide In N,N-dimethyl-formamide at 0 - 20℃; for 18h; |
1
To a solution of 1 -isopropoxy-4-nitrobenzene 1.1 (2 g, 1 1.0 mmol) in DMF(15 mL) was added ./V-chlorosuccinimide (NCS) ( 1.8 g, 13.2 mmol) at 0 0C. After stirring at 0 "C for 4 h, the reaction mixture was allowed to warm to room temperature and stirred for 14 h. The mixture was purified on RP-HPLC using a mixture of acetonitrile and HhO to give 1.2 ( 1.8 g, 76%), which was characterized by 1H NMR. |