Alternatived Products of [ 53015-08-0 ]
Product Details of [ 53015-08-0 ]
CAS No. : | 53015-08-0 |
MDL No. : | MFCD04037449 |
Formula : |
C9H8O4
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
180.16
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 53015-08-0 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 53015-08-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 53015-08-0 ]
- 1
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[ 28281-58-5 ]
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[ 53015-08-0 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 2 steps
2: CrO3; acetic acid / anschliessendes Behandeln mit wss. HCl |
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Stage #1: 7-methoxyisobenzofuran-1(3H)-one With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In benzene at 20 - 85℃; Inert atmosphere;
Stage #2: With water monomer at 100℃; for 1h; |
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Stage #1: 7-methoxyisobenzofuran-1(3H)-one With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In 1,2-dichloro-ethane at 85℃;
Stage #2: With water monomer at 100℃; for 1h; |
|
Reference:
[1]Blair et al.
[Journal of the Chemical Society, 1955, p. 708,711]
[2]He, Yuwei; Cheng, Chuyu; Chen, Bin; Duan, Kun; Zhuang, Yue; Yuan, Bo; Zhang, Meisan; Zhou, Yougui; Zhou, Zihong; Su, Yu-Jun; Cao, Rihui; Qiu, Liqin
[Organic Letters, 2014, vol. 16, # 24, p. 6366 - 6369]
[3]Chen, Li-Na; Ding, Zhi-Jun; Geng, Shu; He, Yuan-Xiang; Hu, Kui; Huang, Feng; Lei, Zhen-Yao; Pan, Li; Zou, Shuai
[Organic and Biomolecular Chemistry, 2022, vol. 20, # 12, p. 2397 - 2401]