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Chemical Structure| 58107-18-9 Chemical Structure| 58107-18-9

Structure of 58107-18-9

Chemical Structure| 58107-18-9

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Product Details of [ 58107-18-9 ]

CAS No. :58107-18-9
Formula : C16H13N3O
M.W : 263.29
SMILES Code : O=C(NC1=CC=CC=C1)NC2=CC=C3N=CC=CC3=C2

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Application In Synthesis of [ 58107-18-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 58107-18-9 ]

[ 58107-18-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 580-15-4 ]
  • [ 103-71-9 ]
  • [ 58107-18-9 ]
YieldReaction ConditionsOperation in experiment
85% In dichloromethane; at 20℃; for 2h; To a solution of amine 6 (3.29 g, 22.8 mmol) in dry dichloromethane (50 mL) was added isocyanate 5 (2.72 g, 22.8 mmol). The reaction mixture was stirred for 2 h at r.t. and the precipitated solid was collected, washed with dichloromethane and hexane, and dried in vacuum to afford 5.15 g of compound EN22 (also called EN02-02) (85 % yield).EN22: 1H NMR (400 MHz, dmso+ccl4) δ 6.99 (t, 1H), 7.30 (t, 2H), 7.45 (dd, 3.9 Hz, 1H), 7.50 (d, 2H), 7.70 (d, 1H), 7.94 (d, 1H), 8.18 (s, 1H), 8.25 (d, 1H), 8.74 (d, 1H), 8.79 (s, 1H), 9.03 (s, 1H).
 

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