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CAS No. : | 587006-12-0 | MDL No. : | MFCD03723862 |
Formula : | C15H11BrN2O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 315.17 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
76% | In water; for 12h;Reflux; | General procedure: The amidoxime (10 mmol) and anhydride (11 mmol) was added to water (20 mL) and the solution was stirred for 12 h at reflux. After stirring, the reaction mixture was washed with diethyl ether (3x50 mL). The resulting mixture was subjected to column chromatography on silica gel with EtOAc/n-hexane (1:9) and evaporation of the solvent under reduced pressure gave pure products in 35-93% yields. All products gave satisfactory spectral data in accord with the assigned structures. |