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[ CAS No. 6021-23-4 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 6021-23-4
Chemical Structure| 6021-23-4
Structure of 6021-23-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 6021-23-4 ]

CAS No. :6021-23-4 MDL No. :MFCD01692499
Formula : C9H14N2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 150.22 Pubchem ID :-
Synonyms :

Safety of [ 6021-23-4 ]

Signal Word: Class:N/A
Precautionary Statements: UN#:N/A
Hazard Statements: Packing Group:N/A

Application In Synthesis of [ 6021-23-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6021-23-4 ]

[ 6021-23-4 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 532-12-7 ]
  • [ 6021-23-4 ]
Reference： [1]Journal of the American Chemical Society,1945,vol. 67,p. 1258,1260
  • 2
  • [ 6021-23-4 ]
  • [ 606-84-8 ]
  • [ 541-41-3 ]
  • 3,3-diphenyl-N-[4-(3-pyridinyl)butyl]-2-propenamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine In tetrahydrofuran 94 3,3-Diphenyl-N-[4-(3-pyridinyl)butyl]-2-propenamide EXAMPLE 94 3,3-Diphenyl-N-[4-(3-pyridinyl)butyl]-2-propenamide To a stirred solution of 3,3-diphenyl-2-propenoic acid (6.23 g), and triethylamine (4.25 mL) in dry tetrahydrofuran (40 mL) at 0° C., was added a solution of ethyl chloroformate (2.74 mL) in tetrahydrofuran (20 mL) dropwise such that the reaction temperature was maintained at 0° C. After the addition was completed, the reaction was stirred at 0° C. for 15 min, then a solution of 3-pyridinebutanamine (4.38 g), in tetrahydrofuran (20 mL) was added dropwise while keeping the reaction at -50° C. The mixture was stirred at 0° C. for 1 hour and then at room temperature for 2 hours before the precipitated triethylamine hydrochloride was removed by filtration. The evaporated filtrate was partitioned between 1N hydrochloric acid solution (80 mL) and ether (80 mL). After the ethereal extract was discarded, the aqueous layer was basified with 4N sodium hydroxide (30 mL) and extracted with ether (4* 100 mL). Evaporation of the dried (K2 CO3) organic extracts afforded 11.1 g of amide which was purified by HPLC (ethyl acetate) to yield 7.42 g of 3,3-diphenyl-N-[4-(3-pyridinyl)butyl]-2-propenamide. A portion was crystallized from ether to give the analytical sample, mp 78°-80° C. Anal. Calculated for C24 H24 N2 O: C, 80.87; H, 6.79; N, 7.86. Found: C, 81.11; H, 6.86; N, 7.89.
Reference： [1]Current Patent Assignee: ROCHE HOLDING AG - US4927838, 1990, A
  • 3
  • [ 6021-23-4 ]
  • [ 118-45-6 ]
  • 4-chloro-2-[[[4-(3-pyridinyl)butyl]amino]carbonyl]benzoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
EXAMPLE 14 4-Chloro-2-[[[4-(3-pyridinyl)butyl]amino]carbonyl]benzoic acid When 5-chlorophthalic anhydride was reacted with 4-(3-pyridinyl)butylamine by the procedure of Example 12, the above compound, mp 152-154 C. was obtained.
Reference： [1]Patent: US4743610,1988,A

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