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[ CAS No. 60789-55-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 60789-55-1
Chemical Structure| 60789-55-1
Structure of 60789-55-1 * Storage: {[proInfo.prStorage]}
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Product Details of [ 60789-55-1 ]

CAS No. :60789-55-1 MDL No. :MFCD09032384
Formula : C13H16O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 188.27 Pubchem ID :-
Synonyms :

Safety of [ 60789-55-1 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 60789-55-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60789-55-1 ]

[ 60789-55-1 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 72517-23-8 ]
  • [ 60789-55-1 ]
  • 5-(6-benzyloxyhexynyl)-2,3-dimethoxybenzoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
62.3% Dissolve 0.6 g (2.3 mmol) of <strong>[72517-23-8]5-bromo-2,3-dimethoxybenzoic acid</strong> in 15 ml of diethylamine, add 8.4 mg of Pd (PPh3) 2Cl2 and 4.4 mg of CuI,After argon gas was purged at 80 C for 30 minutes, a solution of 0.649 g of O-benzyl-5-hexyn-1-ol in Preparation 3 in 2 ml of diethylamine was added dropwise and the mixture was stirred at room temperature for 5 hours and refluxed overnight. The reaction was evaporated to drynessliquid,To the resulting brown residue was added 80 mL of EtOAc, 80 mL of washed with saturated brine and three times of washing. The organic layer was dried over Na2SO4, filtered and evaporated to dryness to give a reddish brown oil.300-400 mesh silica gel preparative separation, the mobile phase of petroleum ether: ethyl acetate = 4: 1, the target component was collected yellow oil 0.527g, yield 62.3%
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