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Chemistry
Heterocyclic Building Blocks
Imidazoles
Bis(1-methyl-1H-imidazol-2-yl)methanone
Chemistry
Heterocyclic Building Blocks
Organic Building Blocks
Imidazoles
Ketones

[ CAS No. 62366-40-9 ] {[proInfo.proName]}

,{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]}
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There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

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Chemical Structure| 62366-40-9
Chemical Structure| 62366-40-9
Structure of 62366-40-9 * Storage: {[proInfo.prStorage]}
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Quality Control of [ 62366-40-9 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 62366-40-9 ]

SDS Specification
Alternatived Products of [ 62366-40-9 ]

Product Details of [ 62366-40-9 ]

CAS No. :62366-40-9 MDL No. :MFCD00956945
Formula : C9H10N4O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 190.20 Pubchem ID :-
Synonyms :

Safety of [ 62366-40-9 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3263
Hazard Statements:H302-H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 62366-40-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 62366-40-9 ]

[ 62366-40-9 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 616-47-7 ]
  • [ 30148-21-1 ]
  • [ 62366-40-9 ]
Reference： [1]Australian Journal of Chemistry,1983,vol. 36,p. 415 - 418
  • 2
  • [ 616-47-7 ]
  • [ 105-58-8 ]
  • [ 62366-40-9 ]
YieldReaction ConditionsOperation in experiment
76% With n-butyllithium In diethyl ether; hexane at -78 - -45℃; for 1.5h;
72% Stage #1: 1-methyl-1H-imidazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: Diethyl carbonate In tetrahydrofuran; hexane at -78 - -40℃; Further stages.;
68% Stage #1: 1-methyl-1H-imidazole With n-butyllithium In tetrahydrofuran; hexane at -45℃; for 0.5h; Stage #2: Diethyl carbonate In tetrahydrofuran; hexane at -80 - -20℃; for 5h;
63% With n-butyllithium In tetrahydrofuran at -78 - -40℃;
47% Stage #1: 1-methyl-1H-imidazole With n-butyllithium In tetrahydrofuran; hexane at -60℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: Diethyl carbonate In tetrahydrofuran; hexane at -60 - 20℃; Inert atmosphere; Schlenk technique;
Stage #1: 1-methyl-1H-imidazole With n-butyllithium In diethyl ether at -65℃; Stage #2: Diethyl carbonate
Stage #1: 1-methyl-1H-imidazole With n-butyllithium In tetrahydrofuran at -45℃; Stage #2: Diethyl carbonate In tetrahydrofuran

Reference： [1]Gorun, Sergiu M.; Papaefthymiou, Georgia C.; Frankel, Richard B.; Lippard, Stephen J. [Journal of the American Chemical Society, 1987, vol. 109, # 14, p. 4244 - 4255]
[2]Collman, James P.; Zhong, Min; Wang, Zhong; Rapta, Miroslav; Rose, Eric [Organic Letters, 1999, vol. 1, # 13, p. 2121 - 2124]
[3]Braussaud; Rüther; Cavell; Skelton; White [Synthesis, 2001, # 4, p. 626 - 632]
[4]Elgafi, Sarah; Field, Leslie D.; Messerle, Barbara A.; Hambley, Trevor W.; Turner, Peter [Journal of the Chemical Society, Dalton Transactions, 1997, # 13, p. 2341 - 2346]
[5]Dauer, David-R.; Koehne, Ingo; Herbst-Irmer, Regine; Stalke, Dietmar [European Journal of Inorganic Chemistry, 2017, vol. 2017, # 13, p. 1966 - 1978]
[6]Burns, Christopher T.; Shen, Han; Jordan, Richard F. [Journal of Organometallic Chemistry, 2003, vol. 683, # 1, p. 240 - 248]
[7]Location in patent: scheme or table Roggan, Stefan; Limberg, Christian; Knispel, Christina; Tilley, T. Don [Dalton Transactions, 2011, vol. 40, # 16, p. 4315 - 4323]
  • 3
  • [ 62366-40-9 ]
  • [ 124225-99-6 ]
YieldReaction ConditionsOperation in experiment
98% With hydrazine hydrate; potassium hydroxide In water at 150℃; for 3h; Inert atmosphere; Schlenk technique;
83% With potassium hydroxide; hydrazine hydrate at 120 - 150℃; for 4h;
39% With sodium hydroxide; hydrazine hydrate at 150℃; for 4h;
reduction;
With potassium hydroxide; hydrazine hydrate at 120 - 150℃;
With hydrazine hydrate; potassium hydroxide at 120 - 150℃;

Reference： [1]Dauer, David-R.; Koehne, Ingo; Herbst-Irmer, Regine; Stalke, Dietmar [European Journal of Inorganic Chemistry, 2017, vol. 2017, # 13, p. 1966 - 1978]
[2]Braussaud; Rüther; Cavell; Skelton; White [Synthesis, 2001, # 4, p. 626 - 632]
[3]Elgafi, Sarah; Field, Leslie D.; Messerle, Barbara A.; Hambley, Trevor W.; Turner, Peter [Journal of the Chemical Society, Dalton Transactions, 1997, # 13, p. 2341 - 2346]
[4]Byers, Peter K.; Canty, Allan J. [Journal of the Chemical Society. Chemical communications, 1988, # 10, p. 639 - 641]
[5]Burns, Christopher T.; Shen, Han; Jordan, Richard F. [Journal of Organometallic Chemistry, 2003, vol. 683, # 1, p. 240 - 248]
[6]Location in patent: scheme or table Roggan, Stefan; Limberg, Christian; Knispel, Christina; Tilley, T. Don [Dalton Transactions, 2011, vol. 40, # 16, p. 4315 - 4323]
  • 4
  • iron(II) tetrafluoroborate hexahydrate [ No CAS ]
  • tetrabutylammonium octacyanidomolybdate(V) [ No CAS ]
  • [ 35487-17-3 ]
  • [ 75-05-8 ]
  • [ 62366-40-9 ]
  • C2H3N*2C4H6N2*C52H40Fe2Mo2N32O4(2-)*2H(1+)*6H2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% at 20℃; for 0.5h;
Reference： [1]Mondal, Abhishake; Li, Yanling; Chamoreau, Lise-Marie; Seuleiman, Mannan; Rechignat, Lionel; Bousseksou, Azzedine; Boillot, Marie-Laure; Lescouezec, Rodrigue [Chemical Communications, 2014, vol. 50, # 22, p. 2893 - 2895]

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