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[ CAS No. 64150-61-4 ] {[proInfo.proName]}

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Chemical Structure| 64150-61-4
Chemical Structure| 64150-61-4
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Product Details of [ 64150-61-4 ]

CAS No. :64150-61-4 MDL No. :MFCD14586276
Formula : C8H4Br2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 275.93 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 64150-61-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 64150-61-4 ]
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[ 64150-61-4 ] Synthesis Path-Upstream   1~3

  • 1
  • [ 496-41-3 ]
  • [ 54008-77-4 ]
  • [ 64150-61-4 ]
Reference: [1] Chemical Science, 2018, vol. 9, # 15, p. 3860 - 3865
  • 2
  • [ 64150-61-4 ]
  • [ 271-89-6 ]
  • [ 59214-70-9 ]
YieldReaction ConditionsOperation in experiment
56% With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran at 23℃; for 0.7 h; Inert atmosphere General procedure: PdCl2(dppf), PdCl2(tbpf) and (A.caPhos)PdCl2. A mixture of the halogenated heterocycle (0.66 mmol) in anhydrous THF (13.2 mL) was degassed by bubbling argon for few minutes. Then, PdCl2(dppf) (27.0 mg, 0.033 mmol, 5.0 molpercent), TMEDA (0.130 g, 1.12 mmol, 1.7 equiv) and finally NaBH4 (42.4 mg, 1.12 mmol, 1.7 equiv) were introduced in sequence. The mixture was stirred at room temperature under argon for the proper time and then worked up as described above.
Reference: [1] Journal of Molecular Catalysis A: Chemical, 2014, vol. 393, p. 191 - 209
  • 3
  • [ 64150-61-4 ]
  • [ 59214-70-9 ]
Reference: [1] Journal of Organic Chemistry, 1996, vol. 61, # 18, p. 6244 - 6251
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