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[ CAS No. 6456-92-4 ] {[proInfo.proName]}

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Chemical Structure| 6456-92-4
Chemical Structure| 6456-92-4
Structure of 6456-92-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 6456-92-4 ]

CAS No. :6456-92-4 MDL No. :
Formula : C7H9NO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 123.15 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 6456-92-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 6456-92-4 ]
  • Downstream synthetic route of [ 6456-92-4 ]

[ 6456-92-4 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 6456-92-4 ]
  • [ 73183-34-3 ]
  • [ 1425045-01-7 ]
YieldReaction ConditionsOperation in experiment
81% With [2,2]bipyridinyl; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer In 1,4-dioxane at 40℃; for 4 h; Inert atmosphere; Schlenk technique General procedure: Ligand (0.010 mmol) and [Ir(OMe)(cod)]2 (3.3 mg, 0.0050 mmol) were placed in a 20-mL two-necked reaction flask, which was filled with N2 by using the standard Schlenk technique. Solvent (0.50 mL) was injected via a syringe, and the mixture was stirred for 5 min at r.t. A solution of 2-pyridone (0.25 mmol) and bis(pinacolato)diboron(0.38–0.75 mmol) in solvent (1.0 mL) was then added, and the suspension was stirred under the indicated conditions. The resulting mixture was allowed to cool to r.t., diluted with EtOAc, and filtered through a short pad of neutral alumina and anhyd Na2SO4. After concentration under reduced pressure, purification by GPC (EtOAc) afforded the corresponding borylated 2-pyridone.
Reference: [1] Synthesis (Germany), 2017, vol. 49, # 21, p. 4745 - 4752
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