There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
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CAS No. : | 65535-53-7 | MDL No. : | MFCD04039913 |
Formula : | C9H8FNO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 165.16 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Danger | Class: | 6.1 |
Precautionary Statements: | P261-P284-P301+P310+P330-P302+P352+P332+P313+P362+P364-P304+P340+P311-P305+P351+P338+P337+P313 | UN#: | 2206 |
Hazard Statements: | H301+H331-H315-H319-H334-H335 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
71% | With triethylamine In toluene Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
77% | With triethylamine In toluene Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
78% | With triethylamine In toluene Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
75% | With triethylamine In toluene Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
69% | With triethylamine In toluene Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
22% | In tetrahydrofuran; at 40 - 45℃; for 24h; | A THF solution (20 ml) of 1- (2-isocyanatoethyl) -4-fluorobenzene (1.51 mmol) and 3-fluoro-4-morpholinoaniline (1.51 mmol)Stir at 40-45 C for 24 hours. The next day, the completion of the reaction was confirmed by TLC. The solvent was distilled off and ammonium chloride (100 ml), water (50 ml) and ethyl acetate (100 ml) were added to the remaining residue. The organic layer was treated with brine and dried over sodium sulfate. The solvent was distilled off and the resulting concentrate was adsorbed onto silica gel using methylene chloride. The mixture was purified by column chromatography using ethyl acetate in hexane to give the title compound. |
22% | In tetrahydrofuran; at 40 - 45℃; for 24h; | A THF solution (20 ml) of 1- (2-isocyanatoethyl) -4-fluorobenzene (1.51 mmol) and 3-fluoro-4-morpholinoaniline (20 ml) 40-45 C. The next day completion of the reaction was confirmed by TLC. The solvent was distilled off and ammonium chloride (100 ml), water (50 ml) and ethyl acetate (100 ml) were added to the remaining residue. Brine organic layer Lt; / RTI & gt; and dried over sodium sulfate. The solvent was distilled off and the resulting concentrate was adsorbed onto silica gel using methylene chloride. The mixture was purified by column chromatography using ethyl acetate in hexane to give the title compound. |