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CAS No. : | 676494-56-7 | MDL No. : | MFCD12923346 |
Formula : | C14H10FNO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 259.23 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1.1: 1,2-dichloro-ethane / 20 °C / Molecular sieve 1.2: 3 h / 20 °C 2.1: Chiralpak AD / N,N-dimethyl-ethanamine; ethanol / Resolution of racemate |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane | ||
Stage #1: 3-fluoro-4-(4-formylphenoxy)benzamide; (2S)-2-(3,5-dimethylphenyl)pyrrolidine In 1,2-dichloro-ethane at 20℃; Molecular sieve; Stage #2: With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 3h; |