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[ CAS No. 681448-78-2 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 681448-78-2
Chemical Structure| 681448-78-2
Structure of 681448-78-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 681448-78-2 ]

CAS No. :681448-78-2 MDL No. :
Formula : C16H12N2O Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 248.28 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 681448-78-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 681448-78-2 ]

[ 681448-78-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 23687-25-4 ]
  • [ 98-88-4 ]
  • [ 681448-78-2 ]
  • 2
  • [ 23687-25-4 ]
  • [ 93-97-0 ]
  • [ 681448-78-2 ]
YieldReaction ConditionsOperation in experiment
With pyridine; at 100℃; for 4h; To a solution of <strong>[23687-25-4]isoquinolin-4-amine</strong> (1.00 g, 6.94 mmol) in pyridine (7 mL) at 25 C under nitrogen, was added benzoic anhydride (1.57 g, 6.94 mmol) in pyridine (1.5 mL). The resulting solution was heated at 100 C for 4 h, then cooled to 25C and quenched using saturated solution of NaHCO3 (5 mL). Crude product was extracted with CHCl3 (5x10 mL). Combined organic phase was washed with water (2x15 mL) and brine (15 mL), then dried over Na2SO4, filtered, and concentrated under reduced pressure to yield the title compound as a purple-red solid (1.66 g, 6.70 mmol, 97% yield) that was used without further purification.
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