Alternatived Products of [ 7145-63-3 ]
Product Details of [ 7145-63-3 ]
CAS No. : | 7145-63-3 |
MDL No. : | |
Formula : |
C14H29NO2
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
243.39
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 7145-63-3 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 7145-63-3 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 7145-63-3 ]
- 1
-
[ 7145-63-3 ]
-
[ 24424-99-5 ]
-
[ 129850-62-0 ]
- 2
-
[ 32986-56-4 ]
-
[ 7145-63-3 ]
-
[ 1300713-56-7 ]
Yield | Reaction Conditions | Operation in experiment |
|
In ethanol; water; at 20 - 40℃; |
General procedure: 1:1 Molar Ratio. TOB-LAA10-11, TOB-LAA12-11, and TOB-LAA14-11, equimolar ion pairs between TOB and the LAA bearing a side alkyl chain of 7, 9, or 11 carbon atoms, respectively (Fig. 1) were prepared by co-evaporation of a co-solution of the two components. TOB base (0.3 mmol) was dissolved in water, while the appropriate LAA (0.3 mmol) was dissolved under magnetic stirring in absolute ethanol. The two solutions were mixed for about 4 h at 40 C and then at overnight room temperature. Ethanol and part of the water were removed under high vacuum at an external temperature of 40 C. Residual water was finally removed by freeze-drying (Edward Modulyo). The resulting fluffy, white powders were stored in tight closed glass vials at 4 +/- 1 C until use.1:3 Molar Ratio. TOB-LAA10-13 and TOB-LAA12-13 were obtained in a similar manner, starting from 0.3 mmol TOB and 0.9 mmol of the chosen LAA.1:5 Molar Ratio. TOB-LAA10-15 and TOB-LAA12-15 were obtained in a similar manner, starting from 0.2 mmol TOB and 1 mmol of the chosen LAA. |