Alternatived Products of [ 72517-22-7 ]
Product Details of [ 72517-22-7 ]
CAS No. : | 72517-22-7 |
MDL No. : | MFCD00475365 |
Formula : |
C9H9ClO4
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
216.62
|
Pubchem ID : | - |
Synonyms : |
|
Safety of [ 72517-22-7 ]
Signal Word: | |
Class: | N/A |
Precautionary Statements: | |
UN#: | N/A |
Hazard Statements: | |
Packing Group: | N/A |
Application In Synthesis of [ 72517-22-7 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 72517-22-7 ]
- 1
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[ 86232-28-2 ]
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[ 72517-22-7 ]
Yield | Reaction Conditions | Operation in experiment |
77% |
With potassium permanganate In water for 5h; Heating; |
|
14% |
With potassium permanganate In water; acetone at 20℃; for 22h; |
|
|
Multi-step reaction with 2 steps
1: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 2) reflux
2: 58 percent / KMnO4 / H2O / 10 h / Heating |
|
Reference:
[1]Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
[Journal of Organic Chemistry USSR (English Translation), 1983, vol. 19, p. 458 - 463][Zhurnal Organicheskoi Khimii, 1983, vol. 19, # 3, p. 522 - 528]
[2]Stark, Daniela; Piel, Markus; Huebner, Harald; Gmeiner, Peter; Gruender, Gerhard; Roesch, Frank
[Bioorganic and Medicinal Chemistry, 2007, vol. 15, # 21, p. 6819 - 6829]
[3]Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
[Journal of Organic Chemistry USSR (English Translation), 1983, vol. 19, p. 458 - 463][Zhurnal Organicheskoi Khimii, 1983, vol. 19, # 3, p. 522 - 528]
- 2
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[ 7740-05-8 ]
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[ 72517-22-7 ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 3 steps
1: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h
2: 75 percent / K2CO3 / acetone / 5 h / Heating
3: 77 percent / KMnO4 / H2O / 5 h / Heating |
|
|
Multi-step reaction with 4 steps
1: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h
2: 75 percent / K2CO3 / acetone / 5 h / Heating
3: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 2) reflux
4: 58 percent / KMnO4 / H2O / 10 h / Heating |
|
|
Multi-step reaction with 3 steps
1: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h
2: 95 percent / KOH (s) / acetone / 8 h / Heating
3: 58 percent / KMnO4 / H2O / 10 h / Heating |
|
Reference:
[1]Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
[Journal of Organic Chemistry USSR (English Translation), 1983, vol. 19, p. 458 - 463][Zhurnal Organicheskoi Khimii, 1983, vol. 19, # 3, p. 522 - 528]
[2]Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
[Journal of Organic Chemistry USSR (English Translation), 1983, vol. 19, p. 458 - 463][Zhurnal Organicheskoi Khimii, 1983, vol. 19, # 3, p. 522 - 528]
[3]Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
[Journal of Organic Chemistry USSR (English Translation), 1983, vol. 19, p. 458 - 463][Zhurnal Organicheskoi Khimii, 1983, vol. 19, # 3, p. 522 - 528]
- 3
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[ 72517-23-8 ]
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[ 72517-22-7 ]