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[ CAS No. 7499-73-2 ] {[proInfo.proName]}

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Chemical Structure| 7499-73-2
Chemical Structure| 7499-73-2
Structure of 7499-73-2 * Storage: {[proInfo.prStorage]}
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CAS No. :7499-73-2 MDL No. :
Formula : C12H9BrN2O3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 309.12 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 7499-73-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 7499-73-2 ]
  • Downstream synthetic route of [ 7499-73-2 ]

[ 7499-73-2 ] Synthesis Path-Upstream   1~3

  • 1
  • [ 7499-73-2 ]
  • [ 74924-94-0 ]
Reference: [1] Journal of Organic Chemistry, 1961, vol. 26, p. 3214 - 3216
[2] Molecular Pharmacology, 2013, vol. 84, # 5, p. 726 - 735
  • 2
  • [ 7499-73-2 ]
  • [ 90767-01-4 ]
YieldReaction ConditionsOperation in experiment
93% With sulfuric acid In ethanol at 20℃; for 4 h; A solution of 1-(acethylamino)-4-bromo-2-nitronaphthalene (535 mg, 1.73 mmol) in 50 percent H2SO4 (10 ml) and EtOH (10 ml) was stirredat ambient temperature for 4hrs. The suspension was washed with diethyl ether. The product(93 percent, orange solid) was filtered and dried in vacuo. 1H – NMR (400 MHz, CDCl3) δ 8.47 (s,1H), 8.23 (d, J = 8.4 Hz, 1H), 7.99 (d, J = 8.4 Hz, 1H), 7.78 (dd, J = 8.2, 7.2 Hz, 1H), 7.65(dd, J = 8.1, 7.3 Hz, 1H), 7.37 (bs, 2H)
Reference: [1] Molecular Pharmacology, 2013, vol. 84, # 5, p. 726 - 735
[2] Justus Liebigs Annalen der Chemie, 1876, vol. 183, p. 250
[3] Journal of the Chemical Society, 1943, p. 321
[4] Justus Liebigs Annalen der Chemie, 1876, vol. 183, p. 250
[5] Journal of the Chemical Society, 1892, vol. 61, p. 769
[6] Chem. News J. Ind. Sci., 1892, vol. 65, p. 59[7] Chemische Berichte, 25 Ref. <1892>,750,
[8] Journal of the Chemical Society, 1885, vol. 47, p. 523[9] Journal of the Chemical Society, 1895, vol. 67, p. 912
[10] Journal of Organic Chemistry, 1961, vol. 26, p. 3214 - 3216
  • 3
  • [ 64-17-5 ]
  • [ 7499-73-2 ]
  • [ 7664-41-7 ]
  • [ 90767-01-4 ]
Reference: [1] Justus Liebigs Annalen der Chemie, 1876, vol. 183, p. 250
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