[ CAS No. 77620-05-4 ] {[proInfo.proName]}

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Quality Control of [ 77620-05-4 ]

COA NMR CNMR HPLC LC-MS

Related Doc. of [ 77620-05-4 ]

SDS Specification

Alternatived Products of [ 77620-05-4 ]

Product Details of [ 77620-05-4 ]

CAS No. :	77620-05-4	MDL No. :	MFCD23098280
Formula :	C₁₀H₁₀O₄	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	-
M.W :	194.18	Pubchem ID :	-
Synonyms :

Safety of [ 77620-05-4 ]

Signal Word:		Class:
Precautionary Statements:		UN#:
Hazard Statements:		Packing Group:

Application In Synthesis of [ 77620-05-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 77620-05-4 ]

[ 77620-05-4 ] Synthesis Path-Downstream 1~32

1
[ 70097-49-3 ]
[ 74-88-4 ]
[ 77620-05-4 ]

Reference： [1]Australian Journal of Chemistry,1981,vol. 34,p. 151 - 162

2
[ 77620-05-4 ]
[ 13925-27-4 ]
[ 77620-08-7 ]

Reference： [1]Australian Journal of Chemistry,1981,vol. 34,p. 151 - 162

3
[ 558-13-4 ]
[ 77620-05-4 ]
[ 215671-88-8 ]

Reference： [1]Tetrahedron Letters,1998,vol. 39,p. 7625 - 7628

4
2-Dimethoxymethyl-5-methoxy-benzoic acid methyl ester [ No CAS ]
[ 77620-05-4 ]

Reference： [1]Tetrahedron Letters,1998,vol. 39,p. 7625 - 7628

5
[ 673-22-3 ]
[ 77620-05-4 ]

Reference： [1]Tetrahedron Letters,1998,vol. 39,p. 7625 - 7628

6
[ 77620-05-4 ]
[ 14963-94-1 ]

Reference： [1]Tetrahedron Letters,1998,vol. 39,p. 7625 - 7628

7
[ 197015-32-0 ]
[ 77620-05-4 ]

Reference： [1]Tetrahedron Letters,1998,vol. 39,p. 7625 - 7628

8
[ 4785-56-2 ]
[ 77-78-1 ]
[ 77620-05-4 ]

Reference： [1]Organic Letters,2014,vol. 16,p. 6366 - 6369
[2]Journal of Organic Chemistry,2010,vol. 75,p. 368 - 374

9
[ 77620-05-4 ]
[ 67-64-1 ]
C₁₃H₁₆O₅ [ No CAS ]

Reference： [1]Journal of Organic Chemistry,2010,vol. 75,p. 368 - 374

10
[ 118-90-1 ]
[ 77620-05-4 ]

Reference： [1]ARKIVOC,2011,vol. 2011,p. 29 - 44

11
[ 1265287-00-0 ]
[ 77620-05-4 ]

Reference： [1]ARKIVOC,2011,vol. 2011,p. 29 - 44

12
[ 578-22-3 ]
[ 77620-05-4 ]

Reference： [1]ARKIVOC,2011,vol. 2011,p. 29 - 44

13
[ 73502-03-1 ]
[ 77620-05-4 ]

Reference： [1]ARKIVOC,2011,vol. 2011,p. 29 - 44

14
[ 3168-59-0 ]
[ 77620-05-4 ]

Reference： [1]ARKIVOC,2011,vol. 2011,p. 29 - 44

15
[ 104-94-9 ]
[ 77620-05-4 ]
[ 67-64-1 ]
2-(4-methoxyphenyl)-6-methoxy-3-(2-oxopropyl)isoindolin-1-one [ No CAS ]

Reference： [1]Synthetic Communications,2012,vol. 42,p. 1115 - 1127

16
[ 4741-63-3 ]
[ 77620-05-4 ]

Reference： [1]Organic Letters,2012,vol. 14,p. 3748 - 3751
[2]Tetrahedron,2013,vol. 69,p. 3287 - 3292
[3]Organic Letters,2014,vol. 16,p. 6366 - 6369
[4]Journal of the American Chemical Society,2018,vol. 140,p. 4860 - 4868

17
[ 4785-56-2 ]
[ 74-88-4 ]
[ 77620-05-4 ]

Yield	Reaction Conditions	Operation in experiment
	With potassium carbonate; In N,N-dimethyl-formamide; for 4h;	General procedure: synthesis of alkyl 2-formylbenzoate. Iodomethane (0.6 mL, 9.5 mmol) was added toa stirred solution of 2-formylbenzoic acid (0.765 g, 5.1 mmol) andpotassium carbonate (0.387 g, 2.8 mmol) in DMF (4 mL). The reactionmixture was refluxed for 4 h, diluted with water (8 mL), andextracted with DCM. The combined organic phases were washedwith 1 N HCl (4 mL), saturated aqueous NaHCO3 (4 mL), and driedover Na2SO4. After filtration and evaporation of the solvents invacuum, the crude product was purified by column chromatographyon silica gel .

Reference： [1]Organic Letters,2012,vol. 14,p. 3748 - 3751
[2]Tetrahedron,2013,vol. 69,p. 3287 - 3292
[3]Journal of the American Chemical Society,2018,vol. 140,p. 4860 - 4868

18
[ 77620-05-4 ]
[ 106-95-6 ]
(S)-3-allyl-6-methoxyisobenzofuran-1(3H)-one [ No CAS ]
[ 1387557-71-2 ]

Reference： [1]Organic Letters,2012,vol. 14,p. 3748 - 3751

19
[ 40125-47-1 ]
[ 77620-05-4 ]

Reference： [1]Organic Letters,2012,vol. 14,p. 3748 - 3751
[2]Journal of the American Chemical Society,2018,vol. 140,p. 4860 - 4868

20
[ 2551-83-9 ]
[ 77620-05-4 ]
(S)-3-allyl-6-methoxyisobenzofuran-1(3H)-one [ No CAS ]
[ 1387557-71-2 ]

Yield	Reaction Conditions	Operation in experiment
55%	With silver fluoride; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; In methanol; at -20℃; for 5h;	2.2.3.6 (R)-3-Allyl-6-methoxyisobenzofuran-1(3H)-one (8f) Representative procedure C was followed. The crude product was purified by column chromatography on silica gel (n-hexane/EtOAc: 1/1) to yield 8f (68.5 mg, 55%). The spectroscopic data was in full agreement with spectral data of an authentic sample. 6 1H NMR (300 MHz, CDCl3): delta=7.36 (s, 1H), 7.33 (d, J=2.1 Hz, 1H), 7.20-7.24 (m, 1H), 5.80-5.69 (m, 1H), 5.47 (t, J=5.9 Hz, 1H), 5.21-5.14 (m, 2H), 3.87 (s, 3H), 2.71-2.57 (m, 2H). 13C NMR (75 MHz, CDCl3): delta=170.5, 160.7, 141.8, 131.3, 127.6, 122.9, 122.9, 119.7, 107.5, 80.1, 55.8, 38.8. [alpha]D20 +19.3 (c 0.4, CHCl3).

Reference： [1]Tetrahedron,2013,vol. 69,p. 3287 - 3292

21
N<SUP>1</SUP>-(2,6-diisopropylbenzyl)ethane-1,2-diamine [ No CAS ]
[ 77620-05-4 ]
1-(2,6-diisopropylbenzyl)-7-methoxy-2,3-dihydro-1H-imidazo[2,1-a]isoindol-5(9bH)-one [ No CAS ]

Reference： [1]Organic Letters,2014,vol. 16,p. 6366 - 6369

22
[ 534-22-5 ]
[ 4248-19-5 ]
[ 77620-05-4 ]
methyl 2-[(tert-butoxycarbonyl)amino](5-methylfuran-2-yl)methyl}-5-methoxybenzoate [ No CAS ]
methyl 2-[bis(5-methylfuran-2-yl)methyl]-5-methoxybenzoate [ No CAS ]