Alternatived Products of [ 84138-75-0 ]
Product Details of [ 84138-75-0 ]
CAS No. : | 84138-75-0 |
MDL No. : | MFCD01590336 |
Formula : |
C10H11N3OS
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
221.28
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 84138-75-0 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 84138-75-0 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 84138-75-0 ]
- 1
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[ 1878-49-5 ]
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[ 79-19-6 ]
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[ 84138-75-0 ]
Yield | Reaction Conditions | Operation in experiment |
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General procedure: A mixture of benzoic acid (50 mmol), N-aminothiourea(50 mmol) and POCl3 (13 mL) was heated at 75 C for 0.5 h. Themixture was cooled to which water (10 mL) was added and thereaction mixture was refluxed for 4 h. The mixture was cooled and pH was adjusted to 8.0 by adding 50% sodium hydroxide solution.The separated solid was filtered and recrystallized from ethanolto give desired compounds. |
Reference:
[1]South African Journal of Chemistry,2010,vol. 63,p. 114 - 122
[2]Journal of Chemical Research,2005,p. 341 - 343
[3]Phosphorus, Sulfur and Silicon and the Related Elements,2006,vol. 181,p. 183 - 190
[4]Chinese Chemical Letters,2010,vol. 21,p. 301 - 304
[5]Bioorganic Chemistry,2015,vol. 59,p. 151 - 167