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[ CAS No. 866787-54-4 ] {[proInfo.proName]}

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Chemical Structure| 866787-54-4
Chemical Structure| 866787-54-4
Structure of 866787-54-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 866787-54-4 ]

CAS No. :866787-54-4 MDL No. :MFCD11977392
Formula : C10H8F3NO4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 263.17 Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 866787-54-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 866787-54-4 ]

[ 866787-54-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 62451-84-7 ]
  • [ 866787-54-4 ]
YieldReaction ConditionsOperation in experiment
34% With trifluoromethylsulfonic anhydride; tetramethylammonium nitrate; In dichloromethane; at 20℃;Heating / reflux; To a solution of (3-Trifluoromethyl-phenyl)-acetic acid methyl ester (14.9 g, 0.068 mol, 1.0 eqiv.) and Me4NNO3 (13.9 g, 0.102 mol, 1.5 eqiv.) in dichloromethane (100 mL) was added dropwise (CF3SO2)2O (28.9 g, 0.102 mol, 1.5 eqiv.) in dichloromethane (50 mL). The mixture was stirred for 2 h at room temperature and heated to reflux overnight. The solution was neutralized with saturated sodium hydrogen carbonate and the organic layer was washed with water. The solution was dried over anhydrous magnesium sulfate and concentrated in vacuo to afford the title compound (6.1 g, 34%) as yellow oil.
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