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CAS No. : | 877766-45-5 | MDL No. : | N/A |
Formula : | C18H11Cl2F3N2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 415.19 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | N/A | |
Precautionary Statements: | UN#: | N/A | |
Hazard Statements: | Packing Group: | N/A |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 8 steps 1.1: dimethyl sulfoxide; sodium chloride / water / 120 °C 2.1: hydrogen / 5% Pd(II)/C(eggshell) / toluene / 20 °C / 760.05 Torr 3.1: tert.-butylnitrite; acetic acid / 2.17 h / 90 - 95 °C / Cooling with ice 4.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetonitrile / 90 °C 5.1: diisobutylaluminium hydride / dichloromethane / 2.25 h / -78 °C / Inert atmosphere 5.2: -78 °C 6.1: manganese(IV) oxide / dichloromethane / 20 °C 7.1: dichloromethane / Reflux 8.1: water; lithium hydroxide / tetrahydrofuran; methanol / 40 °C 8.2: 0 °C / pH 2 | ||
Multi-step reaction with 8 steps 1.1: sodium chloride / water; dimethyl sulfoxide / 16 - 20 h / 120 °C 2.1: hydrogen / 5%-palladium/activated carbon / toluene / 1 - 5 h / 20 °C / 760.05 Torr 3.1: tert.-butylnitrite; acetic acid / 1.83 - 2 h / 90 - 95 °C 4.1: potassium carbonate / tetra-(n-butyl)ammonium iodide / acetonitrile / 1 - 2 h / 90 °C / Heating / reflux 5.1: diisobutylaluminium hydride / dichloromethane / 2 - 2.25 h / -78 °C 5.2: -78 °C 6.1: manganese(IV) oxide / dichloromethane / 0.5 - 3 h / 20 °C 7.1: dichloromethane / 3 - 12 h / Heating / reflux 8.1: methanol; lithium hydroxide; water / tetrahydrofuran / 2 - 3 h / 20 - 40 °C 8.2: 0 °C / pH 2 |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 5 steps 1.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / acetonitrile / 90 °C 2.1: diisobutylaluminium hydride / dichloromethane / 2.25 h / -78 °C / Inert atmosphere 2.2: -78 °C 3.1: manganese(IV) oxide / dichloromethane / 20 °C 4.1: dichloromethane / Reflux 5.1: water; lithium hydroxide / tetrahydrofuran; methanol / 40 °C 5.2: 0 °C / pH 2 | ||
Multi-step reaction with 5 steps 1.1: potassium carbonate / tetra-(n-butyl)ammonium iodide / acetonitrile / 1 - 2 h / 90 °C / Heating / reflux 2.1: diisobutylaluminium hydride / dichloromethane / 2 - 2.25 h / -78 °C 2.2: -78 °C 3.1: manganese(IV) oxide / dichloromethane / 0.5 - 3 h / 20 °C 4.1: dichloromethane / 3 - 12 h / Heating / reflux 5.1: methanol; lithium hydroxide; water / tetrahydrofuran / 2 - 3 h / 20 - 40 °C 5.2: 0 °C / pH 2 |